C₁₀H₁₁F₂N₃

Base Information

Chemical Name:C₁₀H₁₁F₂N₃
CAS No.:1188413-08-2
Molecular Formula:C₁₀H₁₁F₂N₃
Molecular Weight:211.214
Hs Code.:

C<sub>10</sub>H<sub>11</sub>F<sub>2</sub>N<sub>3</sub>

Synonyms:C₁₀H₁₁F₂N₃

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Chemical Property of C₁₀H₁₁F₂N₃

Chemical Property:

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Technology Process of C₁₀H₁₁F₂N₃

There total 6 articles about C₁₀H₁₁F₂N₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1188412-70-5
C₁₁H₁₄F₂O₃S

: 1188413-08-2
C₁₀H₁₁F₂N₃

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 80 ℃; for 2h;

Reference yield:

: 1188412-98-7
1,5-difluoro-2-methyl-3-nitrobenzene

: 1188413-08-2
C₁₀H₁₁F₂N₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogen / palladium 10% on activated carbon / methanol / 2 h / 20 °C / under balloon pressure

2.1: hydrogenchloride / water / 0.17 h / Cooling

2.2: 0.83 h / 0 °C / Cooling with ice

2.3: 1 h / 0 °C

3.1: sec.-butyllithium / tetrahydrofuran; cyclohexane / -100 - -90 °C / Inert atmosphere

3.2: -105 - -90 °C

3.3: -90 - 0 °C

4.1: N-ethyl-N,N-diisopropylamine / dichloromethane / -10 - 20 °C

5.1: sodium azide / N,N-dimethyl-formamide / 2 h / 80 °C

With hydrogenchloride; sodium azide; hydrogen; sec.-butyllithium; N-ethyl-N,N-diisopropylamine; palladium 10% on activated carbon; In tetrahydrofuran; methanol; dichloromethane; cyclohexane; water; N,N-dimethyl-formamide;

Reference yield:

: 452-76-6
2,4-difluorotoluene

: 1188413-08-2
C₁₀H₁₁F₂N₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: sulfuric acid; nitric acid / 2.5 h / 40 - 50 °C

2.1: hydrogen / palladium 10% on activated carbon / methanol / 2 h / 20 °C / under balloon pressure

3.1: hydrogenchloride / water / 0.17 h / Cooling

3.2: 0.83 h / 0 °C / Cooling with ice

3.3: 1 h / 0 °C

4.1: sec.-butyllithium / tetrahydrofuran; cyclohexane / -100 - -90 °C / Inert atmosphere

4.2: -105 - -90 °C

4.3: -90 - 0 °C

5.1: N-ethyl-N,N-diisopropylamine / dichloromethane / -10 - 20 °C

6.1: sodium azide / N,N-dimethyl-formamide / 2 h / 80 °C

With hydrogenchloride; sodium azide; sulfuric acid; hydrogen; sec.-butyllithium; nitric acid; N-ethyl-N,N-diisopropylamine; palladium 10% on activated carbon; In tetrahydrofuran; methanol; dichloromethane; cyclohexane; water; N,N-dimethyl-formamide;