Technology Process of C25H15NO3
There total 7 articles about C25H15NO3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 0.666667h;
DOI:10.1021/ol2025026
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane; water / 1.05 h / 0 - 20 °C
2.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -78 °C
2.2: 0.5 h
3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.67 h / 0 - 20 °C
With
tetrabutyl ammonium fluoride; potassium hexamethylsilazane; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; dichloromethane; water; toluene;
DOI:10.1021/ol2025026
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: acetic acid / ethanol / 14 h / 85 °C
2.1: n-butyllithium / tetrahydrofuran; hexane / 1.17 h / 0 °C
2.2: 0 - 20 °C
2.3: 20 °C
3.1: dichloromethane / 120 h / 20 °C / Acidic conditions
4.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane; water / 1.05 h / 0 - 20 °C
5.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -78 °C
5.2: 0.5 h
6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.67 h / 0 - 20 °C
With
n-butyllithium; tetrabutyl ammonium fluoride; potassium hexamethylsilazane; sodium hydrogencarbonate; acetic acid; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; ethanol; hexane; dichloromethane; water; toluene;
1.1: Fischer indole synthesis;
DOI:10.1021/ol2025026
