5,7a-Di-tert-butyl-3-(2,4,6-trimethyl-phenyl)-3a,7a-dihydro-benzo[d]isoxazole-4,7-dione

Base Information

Chemical Name:5,7a-Di-tert-butyl-3-(2,4,6-trimethyl-phenyl)-3a,7a-dihydro-benzo[d]isoxazole-4,7-dione
CAS No.:89049-50-3
Molecular Formula:C₂₄H₃₁NO₃
Molecular Weight:381.515
Hs Code.:

Synonyms:5,7a-Di-tert-butyl-3-(2,4,6-trimethyl-phenyl)-3a,7a-dihydro-benzo[d]isoxazole-4,7-dione

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Chemical Property of 5,7a-Di-tert-butyl-3-(2,4,6-trimethyl-phenyl)-3a,7a-dihydro-benzo[d]isoxazole-4,7-dione

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Technology Process of 5,7a-Di-tert-butyl-3-(2,4,6-trimethyl-phenyl)-3a,7a-dihydro-benzo[d]isoxazole-4,7-dione

There total 1 articles about 5,7a-Di-tert-butyl-3-(2,4,6-trimethyl-phenyl)-3a,7a-dihydro-benzo[d]isoxazole-4,7-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 2460-77-7
2,5-di-tert-butyl-p-benzoquinone

: 2904-57-6
mesitylenecarbonitrile oxide

: 89049-50-3
5,7a-Di-tert-butyl-3-(2,4,6-trimethyl-phenyl)-3a,7a-dihydro-benzo[d]isoxazole-4,7-dione

Guidance literature:: In benzene; for 720h; Ambient temperature;
DOI:10.1246/bcsj.56.3457

Reference yield: 98.0%

: 89049-50-3
5,7a-Di-tert-butyl-3-(2,4,6-trimethyl-phenyl)-3a,7a-dihydro-benzo[d]isoxazole-4,7-dione

: 145383-58-0
4,7-Di-tert-butyl-4-hydroxy-3-(2,4,6-trimethyl-phenyl)-4H-benzo[d]isoxazol-5-one

Guidance literature:: With sodium hydroxide; In ethanol; for 1h; Ambient temperature;
DOI:10.1246/bcsj.65.2480

Reference yield:

: 89049-50-3
5,7a-Di-tert-butyl-3-(2,4,6-trimethyl-phenyl)-3a,7a-dihydro-benzo[d]isoxazole-4,7-dione

: Acetic acid 5-acetoxy-7-tert-butyl-3-(2,4,6-trimethyl-phenyl)-benzo[d]isoxazol-4-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 10percent NaOH, 2.) dil. HCl / 1.) ethanol

2: 100 percent / H₂SO₄

With hydrogenchloride; sodium hydroxide; sulfuric acid;