Cy₃PAu(1-pyrenyl)

Base Information

• Chemical Name: Cy₃PAu(1-pyrenyl)
• CAS No.: 944940-45-8
• Molecular Formula: C₃₄H₄₂AuP
• Molecular Weight: 678.648
• Mol file: 944940-45-8.mol

Synonyms:Cy₃PAu(1-pyrenyl)

Chemical Property of Cy₃PAu(1-pyrenyl)

Chemical Property:

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Technology Process of Cy₃PAu(1-pyrenyl)

There total 1 articles about Cy₃PAu(1-pyrenyl) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

(tricyclohexylphosphine)gold(I) bromide (49763-42-0) + 1-pyrenylboronic acid (164461-18-1) → Cy3PAu(1-pyrenyl) (944940-45-8)

Guidance literature:

With Cs₂CO₃; In isopropyl alcohol; Au complex added to a suspn. of Cs2CO3 and B compd., stirred at 50°C for 24 h; cooled, evapd. (vac.), extd. (C6H6), filtered, evapd. (vac.), trituratedwith pentane, evapd. (vac.), extd. (C6H6), filtered, concd., crystd. on vapor diffusion of pentane, decanted, recrystd. repeatedly, dried; elem . anal.;

DOI:10.1021/om700346v

upstream raw materials:

(tricyclohexylphosphine)gold(I) bromide

1-pyrenylboronic acid