p-nitrophenyl 4-butyrate

Base Information

• Chemical Name: p-nitrophenyl 4-butyrate
• CAS No.: 129850-47-1
• Molecular Formula: C₂₂H₁₈N₃O₁₁P
• Molecular Weight: 531.372

Synonyms:p-nitrophenyl 4-butyrate

Chemical Property of p-nitrophenyl 4-butyrate

Chemical Property:

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Technology Process of p-nitrophenyl 4-butyrate

There total 1 articles about p-nitrophenyl 4-butyrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C4H6Cl3O2P (200616-64-4) + 4-nitrophenol sodium salt (824-78-2) → p-nitrophenyl 4-butyrate (129850-47-1)

Guidance literature:

In dichloromethane;

Reference yield: 91.0%

Glycine tert-butyl ester (6456-74-2) + p-nitrophenyl 4-butyrate (129850-47-1) → N-(tert-butoxycarbonylmethyl)-4-butyramide (153957-98-3)

Guidance literature:

With dmap; In dichloromethane; for 12h; Ambient temperature;

DOI:10.1055/s-1993-25982

Reference yield: 80.0%

tert-butyl L-alaninate hydrochloride (13404-22-3) + p-nitrophenyl 4-butyrate (129850-47-1) → 2-{4-[bis-(4-nitro-phenoxy)-phosphoryl]-butyrylamino}-propionic acid tert-butyl ester

Guidance literature:

With dmap; In dichloromethane; at 0 ℃; for 5h;

DOI:10.1021/ja0170504

upstream raw materials:

C₄H₆Cl₃O₂P

4-nitrophenol sodium salt

Downstream raw materials:

N-(tert-butoxycarbonylmethyl)-4-butyramide

{4-[Methoxy-(4-nitro-phenoxy)-phosphoryl]-butyrylamino}-acetic acid

N-(carboxymethyl)-4-butyramide

{4-[(2-Fluoro-ethoxy)-(4-nitro-phenoxy)-phosphoryl]-butyrylamino}-acetic acid

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