(E)-N-[4-(3-Amino-propylamino)-butyl]-3-(3-hydroxy-4-methoxy-phenyl)-acrylamide

Base Information

Chemical Name:(E)-N-[4-(3-Amino-propylamino)-butyl]-3-(3-hydroxy-4-methoxy-phenyl)-acrylamide
CAS No.:263245-20-1
Molecular Formula:C₁₇H₂₇N₃O₃
Molecular Weight:321.42
Hs Code.:

Synonyms:(E)-N-[4-(3-Amino-propylamino)-butyl]-3-(3-hydroxy-4-methoxy-phenyl)-acrylamide

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Chemical Property of (E)-N-[4-(3-Amino-propylamino)-butyl]-3-(3-hydroxy-4-methoxy-phenyl)-acrylamide

Chemical Property:

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Technology Process of (E)-N-[4-(3-Amino-propylamino)-butyl]-3-(3-hydroxy-4-methoxy-phenyl)-acrylamide

There total 6 articles about (E)-N-[4-(3-Amino-propylamino)-butyl]-3-(3-hydroxy-4-methoxy-phenyl)-acrylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 219647-35-5
(E)-3-(3-Hydroxy-4-methoxy-phenyl)-N-[4-(tetrahydro-pyrimidin-1-yl)-butyl]-acrylamide

: 263245-20-1
(E)-N-[4-(3-Amino-propylamino)-butyl]-3-(3-hydroxy-4-methoxy-phenyl)-acrylamide

Guidance literature:: With pyridine; malonic acid; In ethanol; for 2h; Heating;
DOI:10.1039/a806688d

Reference yield:

: 621-59-0
isovanillin

: 263245-20-1
(E)-N-[4-(3-Amino-propylamino)-butyl]-3-(3-hydroxy-4-methoxy-phenyl)-acrylamide

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / piperidine, pyridine / ethanol / 3 h / Heating

2: DCC, DMAP / CH₂Cl₂ / 1 h / 25 °C

3: 55 percent / DCC, DMAP / CH₂Cl₂ / -78 - 25 °C

4: 79 percent / malonic acid, pyridine / ethanol / 2 h / Heating

With piperidine; pyridine; dmap; malonic acid; dicyclohexyl-carbodiimide; In ethanol; dichloromethane;
DOI:10.1039/a806688d

Reference yield:

: 124-20-9
N-(3-aminopropyl)-1,4-diaminobutane

: 263245-20-1
(E)-N-[4-(3-Amino-propylamino)-butyl]-3-(3-hydroxy-4-methoxy-phenyl)-acrylamide

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / H₂O / 1 h

2: 55 percent / DCC, DMAP / CH₂Cl₂ / -78 - 25 °C

3: 79 percent / malonic acid, pyridine / ethanol / 2 h / Heating

With pyridine; dmap; malonic acid; dicyclohexyl-carbodiimide; In ethanol; dichloromethane; water;
DOI:10.1039/a806688d