cyclohexyl (S,S)-(+)-3-[2-(methoxymethyl)pyrrolidin-1-ylamino]-3-phenylpropane-1-sulfonate

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Chemical Name:cyclohexyl (S,S)-(+)-3-[2-(methoxymethyl)pyrrolidin-1-ylamino]-3-phenylpropane-1-sulfonate
CAS No.:885678-10-4
Molecular Formula:C₂₁H₃₄N₂O₄S
Molecular Weight:410.578
Hs Code.:

Synonyms:cyclohexyl (S,S)-(+)-3-[2-(methoxymethyl)pyrrolidin-1-ylamino]-3-phenylpropane-1-sulfonate

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Chemical Property of cyclohexyl (S,S)-(+)-3-[2-(methoxymethyl)pyrrolidin-1-ylamino]-3-phenylpropane-1-sulfonate

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Technology Process of cyclohexyl (S,S)-(+)-3-[2-(methoxymethyl)pyrrolidin-1-ylamino]-3-phenylpropane-1-sulfonate

There total 3 articles about cyclohexyl (S,S)-(+)-3-[2-(methoxymethyl)pyrrolidin-1-ylamino]-3-phenylpropane-1-sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3-oxo-propane-1-sulfonic acid cyclohexyl ester

: 885678-10-4
cyclohexyl (S,S)-(+)-3-[2-(methoxymethyl)pyrrolidin-1-ylamino]-3-phenylpropane-1-sulfonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 3.03 g / MgSO₄ / CH₂Cl₂ / 18 h / 20 °C

2.1: CeCl₃ / tetrahydrofuran / 2 h / -78 °C

2.2: 99 percent / tetrahydrofuran / 3 h / -100 - -78 °C

With cerium(III) chloride; magnesium sulfate; In tetrahydrofuran; dichloromethane;
DOI:10.1002/ejoc.200500860

Reference yield:

: 885678-02-4
cyclohexyl but-3-ene-1-sulfonate

: 885678-10-4
cyclohexyl (S,S)-(+)-3-[2-(methoxymethyl)pyrrolidin-1-ylamino]-3-phenylpropane-1-sulfonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: O₃ / CH₂Cl₂ / -78 °C

1.2: PPh₃ / CH₂Cl₂ / 1 h / 20 °C

2.1: 3.03 g / MgSO₄ / CH₂Cl₂ / 18 h / 20 °C

3.1: CeCl₃ / tetrahydrofuran / 2 h / -78 °C

3.2: 99 percent / tetrahydrofuran / 3 h / -100 - -78 °C

With cerium(III) chloride; magnesium sulfate; ozone; In tetrahydrofuran; dichloromethane;
DOI:10.1002/ejoc.200500860

Reference yield:

: 16156-56-2
cyclohexyl mesylate

: 885678-10-4
cyclohexyl (S,S)-(+)-3-[2-(methoxymethyl)pyrrolidin-1-ylamino]-3-phenylpropane-1-sulfonate

Guidance literature:: Multi-step reaction with 4 steps

1.1: nBuLi / tetrahydrofuran / 0.5 h / -78 °C

1.2: 71 percent / tetrahydrofuran / 18 h / -78 - 20 °C

2.1: O₃ / CH₂Cl₂ / -78 °C

2.2: PPh₃ / CH₂Cl₂ / 1 h / 20 °C

3.1: 3.03 g / MgSO₄ / CH₂Cl₂ / 18 h / 20 °C

4.1: CeCl₃ / tetrahydrofuran / 2 h / -78 °C

4.2: 99 percent / tetrahydrofuran / 3 h / -100 - -78 °C

With n-butyllithium; cerium(III) chloride; magnesium sulfate; ozone; In tetrahydrofuran; dichloromethane;
DOI:10.1002/ejoc.200500860