(1R,2R,3R)-N₁-(2-benzyloxy-3-trityloxymethylcyclopentyl)-N₃-((E)-3-methoxyacryloyl)urea

Base Information

• Chemical Name: (1R,2R,3R)-N₁-(2-benzyloxy-3-trityloxymethylcyclopentyl)-N₃-((E)-3-methoxyacryloyl)urea
• CAS No.: 1087192-68-4
• Molecular Formula: C₃₇H₃₈N₂O₅
• Molecular Weight: 590.719

Synonyms:(1R,2R,3R)-N₁-(2-benzyloxy-3-trityloxymethylcyclopentyl)-N₃-((E)-3-methoxyacryloyl)urea

Chemical Property of (1R,2R,3R)-N₁-(2-benzyloxy-3-trityloxymethylcyclopentyl)-N₃-((E)-3-methoxyacryloyl)urea

Chemical Property:

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Technology Process of (1R,2R,3R)-N₁-(2-benzyloxy-3-trityloxymethylcyclopentyl)-N₃-((E)-3-methoxyacryloyl)urea

There total 1 articles about (1R,2R,3R)-N₁-(2-benzyloxy-3-trityloxymethylcyclopentyl)-N₃-((E)-3-methoxyacryloyl)urea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

C6H9NO4 (1087192-66-2) + (1R,2R,3R)-2-benzyloxy-3-trityloxymethylcyclopentamine (1087192-64-0) → (1R,2R,3R)-N1-(2-benzyloxy-3-trityloxymethylcyclopentyl)-N3-((E)-3-methoxyacryloyl)urea (1087192-68-4)

Guidance literature:

With triethylamine; In 1,4-dioxane; at 100 ℃; for 36h; Inert atmosphere;

DOI:10.1021/jo801848h

Reference yield: 69.0%

(1R,2R,3R)-N1-(2-benzyloxy-3-trityloxymethylcyclopentyl)-N3-((E)-3-methoxyacryloyl)urea (1087192-68-4) → (1R,2R,3R)-1-(2-benzyloxy-3-hydroxymethylcyclopentyl)uracil (1087192-71-9)

Guidance literature:

With sulfuric acid; In 1,4-dioxane; water; for 4h; Inert atmosphere; Reflux;

DOI:10.1021/jo801848h

upstream raw materials:

C₆H₉NO₄

(1R,2R,3R)-2-benzyloxy-3-trityloxymethylcyclopentamine

Downstream raw materials:

(1R,2R,3R)-1-(2-benzyloxy-3-hydroxymethylcyclopentyl)uracil

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