4-benzyloxy-3-methoxy-ω-pyrrolidin-2-ylacetophenone

Base Information

Chemical Name:4-benzyloxy-3-methoxy-ω-pyrrolidin-2-ylacetophenone
CAS No.:78178-74-2
Molecular Formula:C₂₀H₂₃NO₃
Molecular Weight:325.408
Hs Code.:

Synonyms:4-benzyloxy-3-methoxy-ω-pyrrolidin-2-ylacetophenone

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Chemical Property of 4-benzyloxy-3-methoxy-ω-pyrrolidin-2-ylacetophenone

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Technology Process of 4-benzyloxy-3-methoxy-ω-pyrrolidin-2-ylacetophenone

There total 2 articles about 4-benzyloxy-3-methoxy-ω-pyrrolidin-2-ylacetophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 5724-81-2
1-pyrroline

: 78178-58-2
4-benzyloxy-3-methoxybenzoylacetic acid

: 78178-74-2
4-benzyloxy-3-methoxy-ω-pyrrolidin-2-ylacetophenone

Guidance literature:: In methanol; water; 1.) cooling, buffered with phosphate to pH 7, 2.) 48h at room temperature;
DOI:10.1016/S0040-4020(01)92028-9

Reference yield:

: 60525-32-8
ethyl 3-[4-(benzyloxy)-3-methoxyphenyl]-3-oxopropanoate

: 78178-74-2
4-benzyloxy-3-methoxy-ω-pyrrolidin-2-ylacetophenone

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent

2: 46 percent / phosphate buffer, pH 7.25-->7.00 / methanol / 60 h / Ambient temperature

With phosphate buffer; In methanol;