Technology Process of C56H69N6O15P
There total 12 articles about C56H69N6O15P which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
at 20 ℃;
for 0.5h;
Inert atmosphere;
DOI:10.1039/c0cc02028a
- Guidance literature:
-
Multi-step reaction with 8 steps
1: pyridine / 20 °C
2: 1H-imidazole / N,N-dimethyl-formamide / 20 °C
3: trifluoroacetic acid / methanol; dichloromethane / 4 h / 0 °C
4: pyridine / 20 °C
5: caesium carbonate / N,N-dimethyl-formamide / 0.5 h / 20 °C
6: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 0.27 h
7: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.17 h / 20 °C
8: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.5 h / 20 °C / Inert atmosphere
With
pyridine; 1H-imidazole; tetrabutyl ammonium fluoride; caesium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/c0cc02028a
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 0.27 h
2: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.17 h / 20 °C
3: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.5 h / 20 °C / Inert atmosphere
With
tetrabutyl ammonium fluoride; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1039/c0cc02028a