C₅₅H₇₈O₁₀Si

Base Information

Chemical Name:C₅₅H₇₈O₁₀Si
CAS No.:1361130-34-8
Molecular Formula:C₅₅H₇₈O₁₀Si
Molecular Weight:927.304
Hs Code.:

C<sub>55</sub>H<sub>78</sub>O<sub>10</sub>Si

Synonyms:C₅₅H₇₈O₁₀Si

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Chemical Property of C₅₅H₇₈O₁₀Si

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Technology Process of C₅₅H₇₈O₁₀Si

There total 23 articles about C₅₅H₇₈O₁₀Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1361130-33-7
C₅₅H₈₀O₁₀Si

: 1361130-34-8
C₅₅H₇₈O₁₀Si

Guidance literature:: With pyridine; Dess-Martin periodane; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1021/ol300182r

Reference yield:

: 1313835-58-3
(5R)-2,2,3,3,9,9,10,10-octamethyl-5-(prop-2-en-1-yl)-4,8-dioxa-3,9-disilaundecane

: 1361130-34-8
C₅₅H₇₈O₁₀Si

Guidance literature:: Multi-step reaction with 12 steps

1.1: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / tetrahydrofuran / 12 h / 20 °C

2.1: sodium periodate / tetrahydrofuran; water / 1 h / 20 °C

3.1: titanium tetrachloride; sparteine / dichloromethane / 0 °C

3.2: 1 h / 0 °C

4.1: 2,6-di-tert-butyl-pyridine / dichloromethane / 18 h / 20 °C

5.1: lithium borohydride / tetrahydrofuran; methanol / 2.5 h / 0 - 20 °C

6.1: Dess-Martin periodane / dichloromethane / 1 h / 0 °C

7.1: chromium dichloride / tetrahydrofuran / 3 h / 20 °C

8.1: chromium dichloride; 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); C₁₇H₂₆N₂O₆S / acetonitrile / 3 h / 20 °C

9.1: palladium 10% on activated carbon; hydrogen / ethanol / 3 h / 35 °C

10.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 38.15 h / 0 - 30 °C

11.1: ammonium fluoride / methanol / 41 h / 20 - 40 °C

12.1: pyridine; Dess-Martin periodane / dichloromethane / 3 h / 20 °C

With pyridine; chromium dichloride; ammonium fluoride; sodium periodate; osmium(VIII) oxide; lithium borohydride; 2,6-di-tert-butyl-pyridine; 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); C₁₇H₂₆N₂O₆S; palladium 10% on activated carbon; water; hydrogen; titanium tetrachloride; Dess-Martin periodane; 4-methylmorpholine N-oxide; N-ethyl-N,N-diisopropylamine; sparteine; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; acetonitrile; 3.1: Evans asymmetric aldol reaction / 3.2: Evans asymmetric aldol reaction / 6.1: Dess-Martin oxidation / 7.1: Takai olefination / 8.1: Nozaki-Hiyama-Kishi reaction / 12.1: Dess-Martin oxidation;
DOI:10.1021/ol300182r

Reference yield:

: 1361130-12-2
C₃₁H₅₅NO₆Si₂

: 1361130-34-8
C₅₅H₇₈O₁₀Si

Guidance literature:: Multi-step reaction with 8 steps

1: lithium borohydride / tetrahydrofuran; methanol / 2.5 h / 0 - 20 °C

2: Dess-Martin periodane / dichloromethane / 1 h / 0 °C

3: chromium dichloride / tetrahydrofuran / 3 h / 20 °C

4: chromium dichloride; 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); C₁₇H₂₆N₂O₆S / acetonitrile / 3 h / 20 °C

5: palladium 10% on activated carbon; hydrogen / ethanol / 3 h / 35 °C

6: N-ethyl-N,N-diisopropylamine / dichloromethane / 38.15 h / 0 - 30 °C

7: ammonium fluoride / methanol / 41 h / 20 - 40 °C

8: pyridine; Dess-Martin periodane / dichloromethane / 3 h / 20 °C

With pyridine; chromium dichloride; ammonium fluoride; lithium borohydride; 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); C₁₇H₂₆N₂O₆S; palladium 10% on activated carbon; hydrogen; Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; ethanol; dichloromethane; acetonitrile; 2: Dess-Martin oxidation / 3: Takai olefination / 4: Nozaki-Hiyama-Kishi reaction / 8: Dess-Martin oxidation;
DOI:10.1021/ol300182r