(E)-(3,4-dimethyl)styryl diphenylphosphine oxide

Base Information

• Chemical Name: (E)-(3,4-dimethyl)styryl diphenylphosphine oxide
• CAS No.: 1310329-66-8
• Molecular Formula: C₂₂H₂₁OP
• Molecular Weight: 332.382
• Mol file: 1310329-66-8.mol

Synonyms:(E)-(3,4-dimethyl)styryl diphenylphosphine oxide

Chemical Property of (E)-(3,4-dimethyl)styryl diphenylphosphine oxide

Chemical Property:

Purity/Quality:

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Technology Process of (E)-(3,4-dimethyl)styryl diphenylphosphine oxide

There total 2 articles about (E)-(3,4-dimethyl)styryl diphenylphosphine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

3-(3,4-Dimethylphenyl)-propensaeure (147219-20-3,60521-25-7) + Diphenylphosphine oxide (4559-70-0) → (E)-(3,4-dimethyl)styryl diphenylphosphine oxide (1310329-66-8)

Guidance literature:

With copper(I) oxide; 1,10-Phenanthroline; silver(l) oxide; In 1-methyl-pyrrolidin-2-one; at 120 ℃; for 6h; regioselective reaction; Inert atmosphere;

DOI:10.1002/chem.201003561

Reference yield: 51.0%

3,4-dimethylstyrene (27831-13-6) + Diphenylphosphine oxide (4559-70-0) → (E)-(3,4-dimethyl)styryl diphenylphosphine oxide (1310329-66-8)

Guidance literature:

With ammonium cerium (IV) nitrate; In 1,4-dioxane; dimethyl sulfoxide; at 40 - 90 ℃; for 12h; Inert atmosphere; Schlenk technique;

DOI:10.1002/ejoc.201900144

upstream raw materials:

3-(3,4-Dimethylphenyl)-propensaeure

Diphenylphosphine oxide

3,4-dimethylstyrene