C₃₇H₈CoF₁₅N₄

Base Information

• Chemical Name: C₃₇H₈CoF₁₅N₄
• CAS No.: 496862-68-1
• Molecular Formula: C₃₇H₈CoF₁₅N₄
• Molecular Weight: 852.467
• Mol file: 496862-68-1.mol

Synonyms:C₃₇H₈CoF₁₅N₄

Chemical Property of C₃₇H₈CoF₁₅N₄

Chemical Property:

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Technology Process of C₃₇H₈CoF₁₅N₄

There total 3 articles about C₃₇H₈CoF₁₅N₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

5,10,15-tris(pentafluorophenyl)corrole → C37H8CoF15N4 (496862-68-1)

Guidance literature:

With cobalt(II) acetate dihydrate; In acetonitrile;

Reference yield: 95.0%

5,10,15-tris(pentafluorophenyl)corrole → [(5,10,15-tris(pentafluorophenyl)corrolato)cobalt(III)] (496862-68-1)

Guidance literature:

With cobalt(II) acetate; In acetonitrile; at 85 - 95 ℃; for 0.333333h; Microwave irradiation;

DOI:10.1021/ja108904s

Reference yield: 95.0%

5,10,15-tris(pentafluorophenyl)corrole + cobalt(II) acetate (71-48-7,917-69-1,5931-89-5,55881-15-7,68931-68-0,68931-69-1,93029-27-7) → [(5,10,15-tris(pentafluorophenyl)corrolato)cobalt(III)] (496862-68-1)

Guidance literature:

In acetonitrile; other Radiation; a microwave glass tube was charged with CH3CN and corrole, the soln. was stirred at room temp. for 10 min, Co-salt was added, stirred for 10 min, sealed, subjected to microwave irradiation at 85°C for 20 min,cooled to room temp.; column chromy. on silica gel (hexane/CH2Cl2 1:1 -> CH2Cl2); elem. anal.;

DOI:10.1021/ja108904s

upstream raw materials:

cobalt(II) acetate