Technology Process of C17H19ClN4O3S
There total 9 articles about C17H19ClN4O3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
1,4-dioxane; dichloromethane;
at 20 ℃;
for 5h;
Product distribution / selectivity;
- Guidance literature:
-
Multi-step reaction with 10 steps
1: dmap / acetonitrile / 16 h / Heating / reflux
2: methanol; potassium carbonate / 16 h / Heating / reflux
3: hydrogen / palladium 10% on activated carbon / ethyl acetate / 16 h
4: isopropyl alcohol / 16 h / Heating / reflux
5: dmap / tetrahydrofuran / 16 h / Heating / reflux
6: hydrazine / ethanol / 3 h
7: dmap; diisopropyl-carbodiimide / chloroform / 0 - 20 °C
8: hydrogenchloride / 1,4-dioxane; dichloromethane / 1 h / 20 °C
9: sodium cyanoborohydride / methanol; N,N-dimethyl-formamide / 16 h / 20 °C
10: hydrogenchloride / 1,4-dioxane; dichloromethane / 5 h / 20 °C
With
hydrogenchloride; methanol; dmap; hydrogen; sodium cyanoborohydride; potassium carbonate; hydrazine; diisopropyl-carbodiimide;
palladium 10% on activated carbon;
In
tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dichloromethane; chloroform; ethyl acetate; N,N-dimethyl-formamide; isopropyl alcohol; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 9 steps
1: methanol; potassium carbonate / 16 h / Heating / reflux
2: hydrogen / palladium 10% on activated carbon / ethyl acetate / 16 h
3: isopropyl alcohol / 16 h / Heating / reflux
4: dmap / tetrahydrofuran / 16 h / Heating / reflux
5: hydrazine / ethanol / 3 h
6: dmap; diisopropyl-carbodiimide / chloroform / 0 - 20 °C
7: hydrogenchloride / 1,4-dioxane; dichloromethane / 1 h / 20 °C
8: sodium cyanoborohydride / methanol; N,N-dimethyl-formamide / 16 h / 20 °C
9: hydrogenchloride / 1,4-dioxane; dichloromethane / 5 h / 20 °C
With
hydrogenchloride; methanol; dmap; hydrogen; sodium cyanoborohydride; potassium carbonate; hydrazine; diisopropyl-carbodiimide;
palladium 10% on activated carbon;
In
tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dichloromethane; chloroform; ethyl acetate; N,N-dimethyl-formamide; isopropyl alcohol;