C₁₅H₂₃NOS

Base Information

Chemical Name:C₁₅H₂₃NOS
CAS No.:1227798-57-3
Molecular Formula:C₁₅H₂₃NOS
Molecular Weight:265.42
Hs Code.:

Synonyms:C₁₅H₂₃NOS

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Chemical Property of C₁₅H₂₃NOS

Chemical Property:

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Technology Process of C₁₅H₂₃NOS

There total 4 articles about C₁₅H₂₃NOS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1227798-54-0
C₁₅H₂₄ClNOS

: 1227798-57-3
C₁₅H₂₃NOS

Guidance literature:: With potassium hydroxide; In tetrahydrofuran; water; for 24h; Reflux;
DOI:10.1039/b925209f

Reference yield:

: C₁₅H₂₄ClNOS

: 1227798-57-3
C₁₅H₂₃NOS

Guidance literature:: With potassium tert-butylate; In isopropyl alcohol; at 50 ℃; for 1h; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/jo4014386

Reference yield:

: 38425-26-2
4-chloro-1-(4-methylphenyl)butan-1-one

: 1227798-57-3
C₁₅H₂₃NOS

Guidance literature:: Multi-step reaction with 3 steps

1: titanium(IV) tetraethanolate / neat (no solvent) / 72 °C / Inert atmosphere

2: [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; 2-Amino-2-methyl-1-propanol; isopropyl alcohol; potassium tert-butylate / 2 h / 50 °C / Molecular sieve; Inert atmosphere

3: potassium tert-butylate / isopropyl alcohol / 1 h / 50 °C / Inert atmosphere

With titanium(IV) tetraethanolate; [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; potassium tert-butylate; 2-Amino-2-methyl-1-propanol; isopropyl alcohol; In isopropyl alcohol;
DOI:10.1021/jo4014386