C₃₁H₃₂F₃NO₆

Base Information

• Chemical Name: C₃₁H₃₂F₃NO₆
• CAS No.: 1597488-12-4
• Molecular Formula: C₃₁H₃₂F₃NO₆
• Molecular Weight: 571.593
• Mol file: 1597488-12-4.mol

Synonyms:C₃₁H₃₂F₃NO₆

Chemical Property of C₃₁H₃₂F₃NO₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₁H₃₂F₃NO₆

There total 3 articles about C₃₁H₃₂F₃NO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

L-vancosaminyl acetate + 3,4-dihydro-9-hydroxy-8-methoxyanthracen-1(2H)-one (79482-37-4) → C31H32F3NO6 (1597488-12-4)

Guidance literature:

With calcium sulfate; trimethylsilyl trifluoromethanesulfonate; In 1,2-dichloro-ethane; at -30 - 10 ℃; for 7h; Inert atmosphere;

DOI:10.1002/anie.201308016

Reference yield:

3-Ethoxycyclohex-2-en-1-one (5323-87-5) → C31H32F3NO6 (1597488-12-4)

Guidance literature:

Multi-step reaction with 2 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C

1.2: 0.33 h / -78 °C

1.3: -78 - 20 °C

2.1: trimethylsilyl trifluoromethanesulfonate; calcium sulfate / 1,2-dichloro-ethane / 7 h / -30 - 10 °C / Inert atmosphere

With calcium sulfate; trimethylsilyl trifluoromethanesulfonate; lithium diisopropyl amide; In tetrahydrofuran; 1,2-dichloro-ethane;

DOI:10.1002/anie.201308016

Reference yield:

methyl 2-methyl-6-methoxybenzoate (79383-44-1) → C31H32F3NO6 (1597488-12-4)

Guidance literature:

Multi-step reaction with 2 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C

1.2: 0.33 h / -78 °C

1.3: -78 - 20 °C

2.1: trimethylsilyl trifluoromethanesulfonate; calcium sulfate / 1,2-dichloro-ethane / 7 h / -30 - 10 °C / Inert atmosphere

With calcium sulfate; trimethylsilyl trifluoromethanesulfonate; lithium diisopropyl amide; In tetrahydrofuran; 1,2-dichloro-ethane;

DOI:10.1002/anie.201308016

upstream raw materials:

3,4-dihydro-9-hydroxy-8-methoxyanthracen-1(2H)-one

methyl 2-methyl-6-methoxybenzoate

3-Ethoxycyclohex-2-en-1-one

Downstream raw materials:

C₃₀H₃₀F₃NO₆

C₄₃H₄₅F₃N₄O₈

C₄₅H₄₆F₆N₂O₉