2-(N-benzoylprop-2-ynylamino)-2-benzylhexa-3,4-dienoic acid methyl ester

Base Information

• Chemical Name: 2-(N-benzoylprop-2-ynylamino)-2-benzylhexa-3,4-dienoic acid methyl ester
• CAS No.: 734547-70-7
• Molecular Formula: C₂₄H₂₃NO₃
• Molecular Weight: 373.452

Synonyms:2-(N-benzoylprop-2-ynylamino)-2-benzylhexa-3,4-dienoic acid methyl ester

Chemical Property of 2-(N-benzoylprop-2-ynylamino)-2-benzylhexa-3,4-dienoic acid methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(N-benzoylprop-2-ynylamino)-2-benzylhexa-3,4-dienoic acid methyl ester

There total 1 articles about 2-(N-benzoylprop-2-ynylamino)-2-benzylhexa-3,4-dienoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

2-benzoylamino-2-benzylhexa-3,4-dienoic acid methyl ester (119839-42-8,119906-50-2,730999-14-1) + propargyl bromide (106-96-7) → 2-(N-benzoylprop-2-ynylamino)-2-benzylhexa-3,4-dienoic acid methyl ester (734547-70-7)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; toluene; at 20 ℃;

DOI:10.1021/ol0492391

Reference yield: 74.0%

2-(N-benzoylprop-2-ynylamino)-2-benzylhexa-3,4-dienoic acid methyl ester (734547-70-7) → 1-benzoyl-2-benzyl-5-methylene-4-vinyl-1,2,5,6-tetrahydropyridine-2-carboxylic acid methyl ester

Guidance literature:

With di(rhodium)tetracarbonyl dichloride; In toluene; at 20 ℃; for 0.166667h;

DOI:10.1021/ol0492391

Reference yield:

2-(N-benzoylprop-2-ynylamino)-2-benzylhexa-3,4-dienoic acid methyl ester (734547-70-7) → 2-benzoyl-1-benzyl-6-ethylidene-5-oxo-1,2,3,5,6,6a-hexahydro-cyclopenta[c]pyrrole-1-carboxylic acid methyl ester + 2-benzoyl-3-benzyl-5-methyl-6-oxo-2,3,5,6-tetrahydro-1H-[2]pyrindine-3-carboxylic acid methyl ester

Guidance literature:

In dimethyl sulfoxide; toluene; at 75 ℃; for 4h; Title compound not separated from byproducts;

DOI:10.1021/ol0492391

upstream raw materials:

2-benzoylamino-2-benzylhexa-3,4-dienoic acid methyl ester

propargyl bromide

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 734547-70-7 2-(N-benzoylprop-2-ynylamino)-2-benzylhexa-3,4-dienoic acid methyl ester

Send

Send

Metric Ton KG G Pound L ML

Send

Send