4-Hydroxy-3-[1-(3-nitro-phenyl)-propyl]-6-phenethyl-6-propyl-5,6-dihydro-pyran-2-one

Base Information

• Chemical Name: 4-Hydroxy-3-[1-(3-nitro-phenyl)-propyl]-6-phenethyl-6-propyl-5,6-dihydro-pyran-2-one
• CAS No.: 174484-97-0
• Molecular Formula: C₂₅H₂₉NO₅
• Molecular Weight: 423.509

Synonyms:4-Hydroxy-3-[1-(3-nitro-phenyl)-propyl]-6-phenethyl-6-propyl-5,6-dihydro-pyran-2-one

Chemical Property of 4-Hydroxy-3-[1-(3-nitro-phenyl)-propyl]-6-phenethyl-6-propyl-5,6-dihydro-pyran-2-one

Chemical Property:

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Technology Process of 4-Hydroxy-3-[1-(3-nitro-phenyl)-propyl]-6-phenethyl-6-propyl-5,6-dihydro-pyran-2-one

There total 2 articles about 4-Hydroxy-3-[1-(3-nitro-phenyl)-propyl]-6-phenethyl-6-propyl-5,6-dihydro-pyran-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-nitro-benzaldehyde (99-61-6) → 4-Hydroxy-3-[1-(3-nitro-phenyl)-propyl]-6-phenethyl-6-propyl-5,6-dihydro-pyran-2-one (174484-97-0)

Guidance literature:

Multi-step reaction with 2 steps

1: AlCl₃ / tetrahydrofuran

2: copper(I) bromide dimethyl sulfide complex / tetrahydrofuran

With aluminium trichloride; copper(I) bromide dimethylsulfide complex; In tetrahydrofuran;

DOI:10.1021/jm960541s

Reference yield:

5,6-dihydro-4-hydroxy-6-phenethyl-6-propyl-2H-pyran-2-one (162174-87-0) → 4-Hydroxy-3-[1-(3-nitro-phenyl)-propyl]-6-phenethyl-6-propyl-5,6-dihydro-pyran-2-one (174484-97-0)

Guidance literature:

Multi-step reaction with 2 steps

1: AlCl₃ / tetrahydrofuran

2: copper(I) bromide dimethyl sulfide complex / tetrahydrofuran

With aluminium trichloride; copper(I) bromide dimethylsulfide complex; In tetrahydrofuran;

DOI:10.1021/jm960541s

Reference yield:

4-Hydroxy-3-[1-(3-nitro-phenyl)-propyl]-6-phenethyl-6-propyl-5,6-dihydro-pyran-2-one (174484-97-0) → 3-[1-(3-Amino-phenyl)-propyl]-4-hydroxy-6-phenethyl-6-propyl-5,6-dihydro-pyran-2-one (174484-99-2)

Guidance literature:

With ammonium formate; palladium on activated charcoal; In methanol;

DOI:10.1021/jm960541s

upstream raw materials:

3-nitro-benzaldehyde

5,6-dihydro-4-hydroxy-6-phenethyl-6-propyl-2H-pyran-2-one

Downstream raw materials:

3-[1-(3-Amino-phenyl)-propyl]-4-hydroxy-6-phenethyl-6-propyl-5,6-dihydro-pyran-2-one

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