6'-(methoxymethyl)-cupreidine 9-O-(4-(perfluoro-n-octyl)benzyl) ether

Base Information

Chemical Name:6'-(methoxymethyl)-cupreidine 9-O-(4-(perfluoro-n-octyl)benzyl) ether
CAS No.:1265816-29-2
Molecular Formula:C₃₆H₃₁F₁₇N₂O₃
Molecular Weight:862.627
Hs Code.:

Synonyms:6'-(methoxymethyl)-cupreidine 9-O-(4-(perfluoro-n-octyl)benzyl) ether

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Chemical Property of 6'-(methoxymethyl)-cupreidine 9-O-(4-(perfluoro-n-octyl)benzyl) ether

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Technology Process of 6'-(methoxymethyl)-cupreidine 9-O-(4-(perfluoro-n-octyl)benzyl) ether

There total 3 articles about 6'-(methoxymethyl)-cupreidine 9-O-(4-(perfluoro-n-octyl)benzyl) ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 882853-72-7
4-(perfluoro-n-octyl)benzyl bromide

: 1265816-25-8
6'-(methoxymethyl)cupreidine

: 1265816-29-2
6'-(methoxymethyl)-cupreidine 9-O-(4-(perfluoro-n-octyl)benzyl) ether

Guidance literature:: 6'-(methoxymethyl)cupreidine; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 2h; Inert atmosphere;

4-(perfluoro-n-octyl)benzyl bromide; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1039/c0gc00619j

Reference yield:

: 524-63-0,70877-75-7
4-[(S)-((2R,4S,5R)-5-ethenyl-1-azabicyclo[2.2.2]octan-2-yl)hydroxymethyl]quinolin-6-ol

: 1265816-29-2
6'-(methoxymethyl)-cupreidine 9-O-(4-(perfluoro-n-octyl)benzyl) ether

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 °C / Inert atmosphere

1.2: 3 h / 20 °C / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 0 °C / Inert atmosphere

2.2: 3 h / 20 °C / Inert atmosphere

With sodium hydride; In N,N-dimethyl-formamide; mineral oil;
DOI:10.1039/c0gc00619j

Reference yield:

: 56-54-2,130-95-0,572-59-8,572-60-1,42151-59-7,47342-58-5,72402-50-7,72402-51-8,72402-52-9,72402-53-0,101143-86-6,101143-87-7,101143-88-8,146925-10-2
quinindine

: 1265816-29-2
6'-(methoxymethyl)-cupreidine 9-O-(4-(perfluoro-n-octyl)benzyl) ether

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium thioethylate / N,N-dimethyl-formamide / 2.5 h / 110 °C / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 °C / Inert atmosphere

2.2: 3 h / 20 °C / Inert atmosphere

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 0 °C / Inert atmosphere

3.2: 3 h / 20 °C / Inert atmosphere

With sodium hydride; sodium thioethylate; In N,N-dimethyl-formamide; mineral oil;
DOI:10.1039/c0gc00619j