C₄₀H₃₄I₂O₁₂

Base Information

• Chemical Name: C₄₀H₃₄I₂O₁₂
• CAS No.: 81707-41-7
• Molecular Formula: C₄₀H₃₄I₂O₁₂
• Molecular Weight: 960.512
• Mol file: 81707-41-7.mol

Synonyms:C₄₀H₃₄I₂O₁₂

Chemical Property of C₄₀H₃₄I₂O₁₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₀H₃₄I₂O₁₂

There total 7 articles about C₄₀H₃₄I₂O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

2,1'-anhydro-6,6'-di-O-mesylsucrose tetrabenzoate (81120-50-5) → C40H34I2O12 (81707-41-7)

Guidance literature:

With sodium iodide; In butanone; at 105 ℃; for 72h;

DOI:10.1016/S0008-6215(00)81039-3

Reference yield:

6,6’-di-O-triphenylmethylsucrose (35674-15-8) → C40H34I2O12 (81707-41-7)

Guidance literature:

Multi-step reaction with 5 steps

1: 45 percent / pyridine / 1.) 0 deg C, 1 h., 2.) room temp., 3 h.

2: M methanolic sodium methoxide / 24 h / Heating

3: pyridine

4: 76 percent / 10percent hydrogen bromide / acetic acid; CHCl₃ / 0.07 h

5: 60 percent / sodium iodide / butan-2-one / 72 h / 105 °C

With pyridine; hydrogen bromide; sodium methylate; sodium iodide; In chloroform; acetic acid; butanone;

DOI:10.1016/S0008-6215(00)81039-3

Reference yield:

C78H64O14 (81076-97-3) → C40H34I2O12 (81707-41-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 76 percent / 10percent hydrogen bromide / acetic acid; CHCl₃ / 0.07 h

2: 60 percent / sodium iodide / butan-2-one / 72 h / 105 °C

With hydrogen bromide; sodium iodide; In chloroform; acetic acid; butanone;

DOI:10.1016/S0008-6215(00)81039-3

upstream raw materials:

2,1'-anhydro-6,6'-di-O-mesylsucrose tetrabenzoate

6,6’-di-O-triphenylmethylsucrose

C₇₈H₆₄O₁₄

benzoyl chloride