(2Z,4E)-3-Dimethylaminomethyl-5-(2,6,6-trimethyl-cyclohex-1-enyl)-penta-2,4-dienenitrile

Base Information

Chemical Name:(2Z,4E)-3-Dimethylaminomethyl-5-(2,6,6-trimethyl-cyclohex-1-enyl)-penta-2,4-dienenitrile
CAS No.:99213-74-8
Molecular Formula:C₁₇H₂₆N₂
Molecular Weight:258.407
Hs Code.:

Synonyms:(2Z,4E)-3-Dimethylaminomethyl-5-(2,6,6-trimethyl-cyclohex-1-enyl)-penta-2,4-dienenitrile

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Chemical Property of (2Z,4E)-3-Dimethylaminomethyl-5-(2,6,6-trimethyl-cyclohex-1-enyl)-penta-2,4-dienenitrile

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Technology Process of (2Z,4E)-3-Dimethylaminomethyl-5-(2,6,6-trimethyl-cyclohex-1-enyl)-penta-2,4-dienenitrile

There total 3 articles about (2Z,4E)-3-Dimethylaminomethyl-5-(2,6,6-trimethyl-cyclohex-1-enyl)-penta-2,4-dienenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2537-48-6
diethyl 1-cyanomethylphosphonate

: 99213-72-6
(dimethylamino)-β-ionone

: (2E,4E)-3-Dimethylaminomethyl-5-(2,6,6-trimethyl-cyclohex-1-enyl)-penta-2,4-dienenitrile

: 99213-74-8
(2Z,4E)-3-Dimethylaminomethyl-5-(2,6,6-trimethyl-cyclohex-1-enyl)-penta-2,4-dienenitrile

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 25 ℃; for 1h; Yield given. Yields of byproduct given;
DOI:10.1021/ja00311a050

Reference yield:

: 79-77-6,14901-07-6
4-(2,6,6-trimethyl-1-cyclohexen-1-yl)-3-buten-2-one

: 99213-74-8
(2Z,4E)-3-Dimethylaminomethyl-5-(2,6,6-trimethyl-cyclohex-1-enyl)-penta-2,4-dienenitrile

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / 5,5-dibromo-2,2-dimethyl-4,6-dioxo-1,3-dioxane / tetrahydrofuran / 2 h / 25 °C

2: 84 percent / sodium carbonate / tetrahydrofuran; H₂O / 1 h / 25 °C

3: NaH / tetrahydrofuran / 1 h / 25 °C

With 2,2-dimethyl-5,5-dibromo-1,3-dioxane-4,6-dione; sodium hydride; sodium carbonate; In tetrahydrofuran; water;
DOI:10.1021/ja00311a050

Reference yield:

: 99213-70-4
bromo-β-ionone

: 99213-74-8
(2Z,4E)-3-Dimethylaminomethyl-5-(2,6,6-trimethyl-cyclohex-1-enyl)-penta-2,4-dienenitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / sodium carbonate / tetrahydrofuran; H₂O / 1 h / 25 °C

2: NaH / tetrahydrofuran / 1 h / 25 °C

With sodium hydride; sodium carbonate; In tetrahydrofuran; water;
DOI:10.1021/ja00311a050