5-[bis(1,2-dihydro-N-methyl-2-oxocyclohepta[b]pyrrol-3-yl)methyl]-3-[bis(1,2-dihydro-2-oxo-N-phenylcyclohepta[b]pyrrol-3-yl)methyl]-1-[bis(2-oxo-2H-cyclohepta[b]furan-3-yl)methyl]benzene

Base Information

• Chemical Name: 5-[bis(1,2-dihydro-N-methyl-2-oxocyclohepta[b]pyrrol-3-yl)methyl]-3-[bis(1,2-dihydro-2-oxo-N-phenylcyclohepta[b]pyrrol-3-yl)methyl]-1-[bis(2-oxo-2H-cyclohepta[b]furan-3-yl)methyl]benzene
• CAS No.: 412310-03-3
• Molecular Formula: C₇₇H₅₂N₄O₈
• Molecular Weight: 1161.28

Synonyms:5-[bis(1,2-dihydro-N-methyl-2-oxocyclohepta[b]pyrrol-3-yl)methyl]-3-[bis(1,2-dihydro-2-oxo-N-phenylcyclohepta[b]pyrrol-3-yl)methyl]-1-[bis(2-oxo-2H-cyclohepta[b]furan-3-yl)methyl]benzene

Chemical Property of 5-[bis(1,2-dihydro-N-methyl-2-oxocyclohepta[b]pyrrol-3-yl)methyl]-3-[bis(1,2-dihydro-2-oxo-N-phenylcyclohepta[b]pyrrol-3-yl)methyl]-1-[bis(2-oxo-2H-cyclohepta[b]furan-3-yl)methyl]benzene

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Technology Process of 5-[bis(1,2-dihydro-N-methyl-2-oxocyclohepta[b]pyrrol-3-yl)methyl]-3-[bis(1,2-dihydro-2-oxo-N-phenylcyclohepta[b]pyrrol-3-yl)methyl]-1-[bis(2-oxo-2H-cyclohepta[b]furan-3-yl)methyl]benzene

There total 4 articles about 5-[bis(1,2-dihydro-N-methyl-2-oxocyclohepta[b]pyrrol-3-yl)methyl]-3-[bis(1,2-dihydro-2-oxo-N-phenylcyclohepta[b]pyrrol-3-yl)methyl]-1-[bis(2-oxo-2H-cyclohepta[b]furan-3-yl)methyl]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

cyclohepta[b]furan-2(2H)-one (4481-35-0) + 3-bis[bis(1,2-dihydro-N-methyl-2-oxocyclohepta[b]pyrrol-3-yl)methyl]-5-[bis(1,2-dihydro-2-oxo-N-phenylcyclohepta[b]pyrrol-3-yl)methyl]benzaldehyde (412310-02-2) → 5-[bis(1,2-dihydro-N-methyl-2-oxocyclohepta[b]pyrrol-3-yl)methyl]-3-[bis(1,2-dihydro-2-oxo-N-phenylcyclohepta[b]pyrrol-3-yl)methyl]-1-[bis(2-oxo-2H-cyclohepta[b]furan-3-yl)methyl]benzene (412310-03-3)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 48h;

DOI:10.1039/b107962j

Reference yield:

1,2-Dihydro-N-methylcyclohepta[b]pyrrol-2-one (3336-87-6) → 5-[bis(1,2-dihydro-N-methyl-2-oxocyclohepta[b]pyrrol-3-yl)methyl]-3-[bis(1,2-dihydro-2-oxo-N-phenylcyclohepta[b]pyrrol-3-yl)methyl]-1-[bis(2-oxo-2H-cyclohepta[b]furan-3-yl)methyl]benzene (412310-03-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 45 percent / TFA / CH₂Cl₂ / 48 h / 20 °C

2: 25 percent / TFA / CH₂Cl₂ / 48 h / 20 °C

3: 97 percent / TFA / CH₂Cl₂ / 48 h / 20 °C

With trifluoroacetic acid; In dichloromethane;

DOI:10.1039/b107962j

Reference yield:

benzene-1,3,5-trialdehyde (3163-76-6) → 5-[bis(1,2-dihydro-N-methyl-2-oxocyclohepta[b]pyrrol-3-yl)methyl]-3-[bis(1,2-dihydro-2-oxo-N-phenylcyclohepta[b]pyrrol-3-yl)methyl]-1-[bis(2-oxo-2H-cyclohepta[b]furan-3-yl)methyl]benzene (412310-03-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 45 percent / TFA / CH₂Cl₂ / 48 h / 20 °C

2: 25 percent / TFA / CH₂Cl₂ / 48 h / 20 °C

3: 97 percent / TFA / CH₂Cl₂ / 48 h / 20 °C

With trifluoroacetic acid; In dichloromethane;

DOI:10.1039/b107962j

upstream raw materials:

cyclohepta[b]furan-2(2H)-one

3-bis[bis(1,2-dihydro-N-methyl-2-oxocyclohepta[b]pyrrol-3-yl)methyl]-5-[bis(1,2-dihydro-2-oxo-N-phenylcyclohepta[b]pyrrol-3-yl)methyl]benzaldehyde

1,2-Dihydro-N-methylcyclohepta[b]pyrrol-2-one

benzene-1,3,5-trialdehyde

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