C₁₅H₁₀OS

Base Information

• Chemical Name: C₁₅H₁₀OS
• CAS No.: 1558818-57-7
• Molecular Formula: C₁₅H₁₀OS
• Molecular Weight: 238.31
• Mol file: 1558818-57-7.mol

Synonyms:C₁₅H₁₀OS

Chemical Property of C₁₅H₁₀OS

Chemical Property:

Purity/Quality:

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• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₁₅H₁₀OS

There total 1 articles about C₁₅H₁₀OS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

2-Iodothiophene (3437-95-4,149762-92-5) + 3-(2-ethynylphenyl)-2-propyn-1-ol (157406-24-1) → C15H10OS (1558818-57-7)

Guidance literature:

2-Iodothiophene; With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; at 30 ℃; for 0.5h; Inert atmosphere;

3-(2-ethynylphenyl)-2-propyn-1-ol; at 30 ℃; for 3h; Inert atmosphere;

DOI:10.1039/c3ob41911h

Reference yield: 70.0%

anthranil (271-58-9) + C15H10OS (1558818-57-7) → 1-((2-formylphenyl)amino)-3-(thiophen-2-yl)-2-naphthaldehyde

Guidance literature:

With 2-(di-tert-butylphosphino)-1,1'-biphenylgold(I) chloride; silver(I) triflimide; In 1,2-dichloro-ethane; at 80 ℃; for 36h; chemoselective reaction; Inert atmosphere;

DOI:10.1002/adsc.202000591

Reference yield: 53.0%

C15H10OS (1558818-57-7) + 1,3-cylohexanedione (504-02-9) → C21H16O2S (1558818-37-3)

Guidance literature:

With iron(III) p-toluenesulfonate hexahydrate; In 1,2-dichloro-ethane; at 80 ℃; for 24h; Inert atmosphere;

DOI:10.1039/c3ob41911h

upstream raw materials:

2-Iodothiophene

3-(2-ethynylphenyl)-2-propyn-1-ol

Downstream raw materials:

C₂₁H₁₆O₂S