4-Methylumbelliferylbeta-D-ribofuranoside

Base Information

• Chemical Name: 4-Methylumbelliferylbeta-D-ribofuranoside
• CAS No.: 195385-93-4
• Molecular Formula: C15H16O7
• Molecular Weight: 308.28300
• Hs Code.: 2932190090
• Mol file: 195385-93-4.mol

Synonyms:

Chemical Property of 4-Methylumbelliferylbeta-D-ribofuranoside

Chemical Property:

• Vapor Pressure: 3.24E-15mmHg at 25°C
• Melting Point: 165-170°C
• Boiling Point: 599.4oC at 760 mmHg
• PKA: 12.95±0.70(Predicted)
• Flash Point: 228.1oC
• PSA: 109.36000
• Density: 1.486g/cm3
• LogP: -0.08080
• Storage Temp.: Refrigerator, under inert atmosphere
• Solubility.: Chloroform (Slightly), DMSO (Slightly)

Purity/Quality:

98% ^*data from raw suppliers

4-Methylumbelliferyl b-D-ribofuranoside ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-Methylumbelliferylbeta-D-ribofuranoside

There total 9 articles about 4-Methylumbelliferylbeta-D-ribofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

4′-methylumbelliferyl 2,3,5-tri-O-acetyl-β-D-ribofuranoside → 4-methylumbelliferyl β-D-ribofuranoside (195385-93-4)

Guidance literature:

With potassium hydroxide; In methanol; at 20 ℃; for 0.416667h;

DOI:10.3390/molecules201219789

Reference yield: 47.0%

→ 4-methylumbelliferyl β-D-ribofuranoside (195385-93-4)

Guidance literature:

Reference yield: 10.0%

4-methylumbelliferyl 2,3,5-tri-O-benzoyl-α-L-arabinofuranoside (106488-03-3,113728-14-6,195385-92-3) → 7-hydroxy-4-methylcoumarin-7-yl α-L-arabinofuranoside (77471-44-4,195385-93-4)

Guidance literature:

With ammonia; In methanol; at 4 ℃; for 72h;

DOI:10.1016/0008-6215(88)84045-X

upstream raw materials:

4-methylumbelliferyl 2,3,5-tri-O-benzoyl-α-L-arabinofuranoside

β-7-hydroxy-4-methylcoumarin-7-yl D-galactofuranoside

7-hydroxy-4-methyl-chromen-2-one

7-hydroxy-4-methyl-2-oxo-2H-1-benzopyran tetrabutylammonium salt

Refernces

• 1、 -. "Based on 4 - methyl [...] synthesis method of a plurality of glycoside". Paragraph 0088; 0089. . Retrieved 2018/10/11.
• 2、 -. "ENZYME DETECTION/ASSAY METHOD AND SUBSTRATES". . . Retrieved 2008/06/13.