C₃₂H₃₃N₇O₃

Base Information

Chemical Name:C₃₂H₃₃N₇O₃
CAS No.:1228968-51-1
Molecular Formula:C₃₂H₃₃N₇O₃
Molecular Weight:563.659
Hs Code.:

C<sub>32</sub>H<sub>33</sub>N<sub>7</sub>O<sub>3</sub>

Synonyms:C₃₂H₃₃N₇O₃

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Chemical Property of C₃₂H₃₃N₇O₃

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Technology Process of C₃₂H₃₃N₇O₃

There total 11 articles about C₃₂H₃₃N₇O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1228968-50-0
C₃₅H₃₄Cl₃N₇O₅

: 1228968-51-1
C₃₂H₃₃N₇O₃

Guidance literature:: C₃₅H₃₄Cl₃N₇O₅; With acetic acid; zinc; at 50 ℃; for 4h;

With sodium hydrogencarbonate; In tetrahydrofuran; water; pH=8;

Reference yield:

: 69610-41-9,117625-90-8
Boc-L-Pro-H

: 1228968-51-1
C₃₂H₃₃N₇O₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: ammonium hydroxide / methanol; water / 20 °C

2.1: N-iodo-succinimide / dichloromethane / 1 h / 0 °C

3.1: water; sodium sulfite / ethanol / 17 h / Reflux

4.1: triethylamine / dmap / dichloromethane / 2 h / 20 °C

5.1: N-ethyl-N,N-diisopropylamine / bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / tetrahydrofuran / 2 h / 20 °C

6.1: hydrogenchloride / 1,4-dioxane / 3 h / 20 °C

7.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 1 h / 20 °C

8.1: acetic acid; zinc / 4 h / 50 °C

8.2: pH 8

With hydrogenchloride; ammonium hydroxide; N-iodo-succinimide; water; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; HATU; sodium sulfite; zinc; dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 1007882-58-7,1332326-40-5
(S)-tert-butyl 2-(1H-imidazol-2-yl)pyrrolidine-1-carboxylate

: 1228968-51-1
C₃₂H₃₃N₇O₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: N-iodo-succinimide / dichloromethane / 1 h / 0 °C

2.1: water; sodium sulfite / ethanol / 17 h / Reflux

3.1: triethylamine / dmap / dichloromethane / 2 h / 20 °C

4.1: N-ethyl-N,N-diisopropylamine / bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / tetrahydrofuran / 2 h / 20 °C

5.1: hydrogenchloride / 1,4-dioxane / 3 h / 20 °C

6.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 1 h / 20 °C

7.1: acetic acid; zinc / 4 h / 50 °C

7.2: pH 8

With hydrogenchloride; N-iodo-succinimide; water; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; HATU; sodium sulfite; zinc; dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; N,N-dimethyl-formamide;