2-[5-(2-azidopropyl)tetrahydrofuran-2-yl]propionic acid 1-(tert-butyldiphenylsilanyloxymethyl)allyl ester

Base Information

Chemical Name:2-[5-(2-azidopropyl)tetrahydrofuran-2-yl]propionic acid 1-(tert-butyldiphenylsilanyloxymethyl)allyl ester
CAS No.:1263474-71-0
Molecular Formula:C₃₀H₄₁N₃O₄Si
Molecular Weight:535.759
Hs Code.:

Synonyms:2-[5-(2-azidopropyl)tetrahydrofuran-2-yl]propionic acid 1-(tert-butyldiphenylsilanyloxymethyl)allyl ester

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Chemical Property of 2-[5-(2-azidopropyl)tetrahydrofuran-2-yl]propionic acid 1-(tert-butyldiphenylsilanyloxymethyl)allyl ester

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Technology Process of 2-[5-(2-azidopropyl)tetrahydrofuran-2-yl]propionic acid 1-(tert-butyldiphenylsilanyloxymethyl)allyl ester

There total 4 articles about 2-[5-(2-azidopropyl)tetrahydrofuran-2-yl]propionic acid 1-(tert-butyldiphenylsilanyloxymethyl)allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 8-azidononactic acid chloride

: 91376-49-7
(S)-1-(tert-butyldiphenylsilyloxy)-2-hydroxy-3-butene

: 1263474-71-0
2-[5-(2-azidopropyl)tetrahydrofuran-2-yl]propionic acid 1-(tert-butyldiphenylsilanyloxymethyl)allyl ester

Guidance literature:: With 4-methyl-morpholine; dmap; In dichloromethane; at 0 - 20 ℃; for 7h; Inert atmosphere;
DOI:10.3998/ark.5550190.0012.513

Reference yield:

: 1263474-69-6
2-[5-(2-azidopropyl)tetrahydrofuran-2-yl]propionic acid methyl ester

: 1263474-71-0
2-[5-(2-azidopropyl)tetrahydrofuran-2-yl]propionic acid 1-(tert-butyldiphenylsilanyloxymethyl)allyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydroxide / tetrahydrofuran; methanol / 20 h / 20 °C

2: oxalyl dichloride / benzene / 6 h / 20 °C

3: 4-methyl-morpholine; dmap / dichloromethane / 7 h / 0 - 20 °C / Inert atmosphere

With 4-methyl-morpholine; dmap; oxalyl dichloride; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; benzene;
DOI:10.3998/ark.5550190.0012.513

Reference yield:

: 1263474-70-9
2-[5-(2-azidopropyl)tetrahydrofuran-2-yl]propionic acid

: 1263474-71-0
2-[5-(2-azidopropyl)tetrahydrofuran-2-yl]propionic acid 1-(tert-butyldiphenylsilanyloxymethyl)allyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride / benzene / 6 h / 20 °C

2: 4-methyl-morpholine; dmap / dichloromethane / 7 h / 0 - 20 °C / Inert atmosphere

With 4-methyl-morpholine; dmap; oxalyl dichloride; In dichloromethane; benzene;
DOI:10.3998/ark.5550190.0012.513