5-(methylthio)-3,7-dioxo-1-(4-methoxybenzyl)-2-oxa-4,6,8-triazanon-4-en-9-oic acid methyl ester

Base Information

Chemical Name:5-(methylthio)-3,7-dioxo-1-(4-methoxybenzyl)-2-oxa-4,6,8-triazanon-4-en-9-oic acid methyl ester
CAS No.:1353585-33-7
Molecular Formula:C₁₃H₁₇N₃O₄S
Molecular Weight:311.362
Hs Code.:

Synonyms:5-(methylthio)-3,7-dioxo-1-(4-methoxybenzyl)-2-oxa-4,6,8-triazanon-4-en-9-oic acid methyl ester

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Chemical Property of 5-(methylthio)-3,7-dioxo-1-(4-methoxybenzyl)-2-oxa-4,6,8-triazanon-4-en-9-oic acid methyl ester

Chemical Property:

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Technology Process of 5-(methylthio)-3,7-dioxo-1-(4-methoxybenzyl)-2-oxa-4,6,8-triazanon-4-en-9-oic acid methyl ester

There total 2 articles about 5-(methylthio)-3,7-dioxo-1-(4-methoxybenzyl)-2-oxa-4,6,8-triazanon-4-en-9-oic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (((4-methoxybenzyl)amino)carbonyl)carbamimidothioic acid methyl ester

: 79-22-1
methyl chloroformate

: 1353585-33-7
5-(methylthio)-3,7-dioxo-1-(4-methoxybenzyl)-2-oxa-4,6,8-triazanon-4-en-9-oic acid methyl ester

Guidance literature:: With triethylamine; In dichloromethane; at -10 - 20 ℃;
DOI:10.1016/j.bmcl.2009.03.157

Reference yield:

: 56651-60-6
4-methoxybenzyl isocyanate

: 1353585-33-7
5-(methylthio)-3,7-dioxo-1-(4-methoxybenzyl)-2-oxa-4,6,8-triazanon-4-en-9-oic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / water; tetrahydrofuran; methanol / 0 - 20 °C

2: triethylamine / dichloromethane / 4.25 h / -10 - 20 °C

With triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water;

Reference yield:

: 1353585-33-7
5-(methylthio)-3,7-dioxo-1-(4-methoxybenzyl)-2-oxa-4,6,8-triazanon-4-en-9-oic acid methyl ester

: 3-(4-methoxybenzyl)-6-methylsulfanyl-1H-[1,3,5]-triazine-2,4-dione hydrochloride

Guidance literature:: 5-(methylthio)-3,7-dioxo-1-(4-methoxybenzyl)-2-oxa-4,6,8-triazanon-4-en-9-oic acid methyl ester; With sodium methylate; In methanol; at 20 ℃; for 1h;

With hydrogenchloride; In methanol; water;