[ ETHVL-2-METHYL-2-R₂-METHYL-4-(N-(3-METHOXVPROPVL) AMINOMETHVL) PHENOXYL-] propanoate

Base Information

• Chemical Name: [ ETHVL-2-METHYL-2-R₂-METHYL-4-(N-(3-METHOXVPROPVL) AMINOMETHVL) PHENOXYL-] propanoate
• CAS No.: 639784-54-6
• Molecular Formula: C₁₈H₂₉NO₄
• Molecular Weight: 323.433

Synonyms:[ ETHVL-2-METHYL-2-R₂-METHYL-4-(N-(3-METHOXVPROPVL) AMINOMETHVL) PHENOXYL-] propanoate

Chemical Property of [ ETHVL-2-METHYL-2-R₂-METHYL-4-(N-(3-METHOXVPROPVL) AMINOMETHVL) PHENOXYL-] propanoate

Chemical Property:

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Technology Process of [ ETHVL-2-METHYL-2-R₂-METHYL-4-(N-(3-METHOXVPROPVL) AMINOMETHVL) PHENOXYL-] propanoate

There total 2 articles about [ ETHVL-2-METHYL-2-R₂-METHYL-4-(N-(3-METHOXVPROPVL) AMINOMETHVL) PHENOXYL-] propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.15%

2-(4-FORMYL-2-METHYL-PHENOXY)-2-METHYL-PROPIONIC acid ethyl ester (637352-45-5) → [ ETHVL-2-METHYL-2-R2-METHYL-4-(N-(3-METHOXVPROPVL) AMINOMETHVL) PHENOXYL-] propanoate (639784-54-6)

Guidance literature:

With sodium triacetoxy borohydride; trifluoroethylamine; In dichloromethane; at 25 ℃; for 1h;

Reference yield:

4-hydroxy-3-methyl-benzaldehyde (15174-69-3) → [ ETHVL-2-METHYL-2-R2-METHYL-4-(N-(3-METHOXVPROPVL) AMINOMETHVL) PHENOXYL-] propanoate (639784-54-6)

Guidance literature:

Multi-step reaction with 2 steps

1: ethyl 2-bromoisobutyrate / 36 h

2: sodium triacetoxy borohydride; trifluoroethylamine / dichloromethane / 1 h / 25 °C

With ethyl 2-bromoisobutyrate; sodium triacetoxy borohydride; trifluoroethylamine; In dichloromethane;

Reference yield: 98.72%

[ ETHVL-2-METHYL-2-R2-METHYL-4-(N-(3-METHOXVPROPVL) AMINOMETHVL) PHENOXYL-] propanoate (639784-54-6) → Example 48

Guidance literature:

With potassium carbonate; 5-(chloromethyl)-4-methyl-2-[4-(trifluoromethyl)phenyl]-1,3-thiazole; for 1h;

upstream raw materials:

2-(4-FORMYL-2-METHYL-PHENOXY)-2-METHYL-PROPIONIC acid ethyl ester

4-hydroxy-3-methyl-benzaldehyde

Downstream raw materials:

2-methyl-2-[2-methyl-4-{[(4-methyl-2-[4-trifluoromethylphenyl]-thiazol-5-YLMETHYL)-N-(3-METHOXYPROPYL)-AMINO]METHYL}PHENOXY]PROPIONIC ACID

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