1-benzyl-3-formyl-9-methoxy-1H-benzindole

Base Information

Chemical Name:1-benzyl-3-formyl-9-methoxy-1H-benzindole
CAS No.:151646-90-1
Molecular Formula:C₂₁H₁₇NO₂
Molecular Weight:315.371
Hs Code.:

1-benzyl-3-formyl-9-methoxy-1H-benz<f>indole

Synonyms:1-benzyl-3-formyl-9-methoxy-1H-benzindole

Suppliers and Price of 1-benzyl-3-formyl-9-methoxy-1H-benzindole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 1-benzyl-3-formyl-9-methoxy-1H-benzindole

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of 1-benzyl-3-formyl-9-methoxy-1H-benzindole

There total 3 articles about 1-benzyl-3-formyl-9-methoxy-1H-benzindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 151646-89-8
1-benzyl-9-methoxy-1H-benzindole

: 151646-90-1
1-benzyl-3-formyl-9-methoxy-1H-benzindole

Guidance literature:: With trichlorophosphate; at 0 ℃; for 0.5h;
DOI:10.1002/jhet.5570300137

Reference yield:

: 121045-66-7
ethyl 1-benzyl-9-methoxy-1H-benzindole-2-carboxylate

: 151646-90-1
1-benzyl-3-formyl-9-methoxy-1H-benzindole

Guidance literature:: Multi-step reaction with 3 steps

1: KOH / ethanol / 0.5 h / Heating

2: copper chromite / quinoline / 0.25 h / 200 °C

3: 69 percent / phosphoryl chloride / 0.5 h / 0 °C

With potassium hydroxide; copper chromite; trichlorophosphate; In quinoline; ethanol;
DOI:10.1002/jhet.5570300137

Reference yield:

: 1-benzyl-9-methoxy-1H-benzindole-2-carboxylic acid

: 151646-90-1
1-benzyl-3-formyl-9-methoxy-1H-benzindole

Guidance literature:: Multi-step reaction with 2 steps

1: copper chromite / quinoline / 0.25 h / 200 °C

2: 69 percent / phosphoryl chloride / 0.5 h / 0 °C

With copper chromite; trichlorophosphate; In quinoline;
DOI:10.1002/jhet.5570300137