methyl 3-O-benzyl-4,6-O-benzylidene-2-O-[(4-O-benzoyl-3-O-benzyl-2-O-(2-trifluoromethylbenzenesulfonyl)-β-L-rhamnopyranosyl)]-α-D-mannopyranoside

Base Information

Chemical Name:methyl 3-O-benzyl-4,6-O-benzylidene-2-O-[(4-O-benzoyl-3-O-benzyl-2-O-(2-trifluoromethylbenzenesulfonyl)-β-L-rhamnopyranosyl)]-α-D-mannopyranoside
CAS No.:503066-02-2
Molecular Formula:C₄₈H₄₇F₃O₁₃S
Molecular Weight:920.955
Hs Code.:

methyl 3-O-benzyl-4,6-O-benzylidene-2-O-[(4-O-benzoyl-3-O-benzyl-2-O-(2-trifluoromethylbenzenesulfonyl)-β-L-rhamnopyranosyl)]-α-D-mannopyranoside

Synonyms:methyl 3-O-benzyl-4,6-O-benzylidene-2-O-[(4-O-benzoyl-3-O-benzyl-2-O-(2-trifluoromethylbenzenesulfonyl)-β-L-rhamnopyranosyl)]-α-D-mannopyranoside

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Chemical Property of methyl 3-O-benzyl-4,6-O-benzylidene-2-O-[(4-O-benzoyl-3-O-benzyl-2-O-(2-trifluoromethylbenzenesulfonyl)-β-L-rhamnopyranosyl)]-α-D-mannopyranoside

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Technology Process of methyl 3-O-benzyl-4,6-O-benzylidene-2-O-[(4-O-benzoyl-3-O-benzyl-2-O-(2-trifluoromethylbenzenesulfonyl)-β-L-rhamnopyranosyl)]-α-D-mannopyranoside

There total 2 articles about methyl 3-O-benzyl-4,6-O-benzylidene-2-O-[(4-O-benzoyl-3-O-benzyl-2-O-(2-trifluoromethylbenzenesulfonyl)-β-L-rhamnopyranosyl)]-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 358-23-6
trifluoromethylsulfonic anhydride

: 2774-19-8,14419-69-3,15887-67-9,23392-28-1,57539-08-9,61277-63-2,74410-51-8,76419-48-2,80734-73-2,86363-44-2,89301-79-1,94061-92-4,94062-87-0,108739-92-0,129706-93-0,143005-12-3,65877-21-6
(2R,4aR,6S,7S,8R,8aR)-8-Benzyloxy-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-ol

: 503065-97-2
phenyl 4-O-benzoyl-3-O-benzyl-2-O-(2-trifluoromethylbenzenesulfonyl)-1-thio-β-L-rhamnopyranoside

: 503066-02-2
methyl 3-O-benzyl-4,6-O-benzylidene-2-O-[(4-O-benzoyl-3-O-benzyl-2-O-(2-trifluoromethylbenzenesulfonyl)-β-L-rhamnopyranosyl)]-α-D-mannopyranoside

: methyl 3-O-benzyl-4,6-O-benzylidene-2-O-[(4-O-benzoyl-3-O-benzyl-2-O-(2-trifluoromethylbenzenesulfonyl)-α-L-rhamnopyranosyl)]-α-D-mannopyranoside

Guidance literature:: trifluoromethylsulfonic anhydride; phenyl 4-O-benzoyl-3-O-benzyl-2-O-(2-trifluoromethylbenzenesulfonyl)-1-thio-β-L-rhamnopyranoside; With 1-benzenesulfinyl piperidine; 2,4,6-tri-tert-butylpyrimidine; In dichloromethane; at -60 ℃; for 1h;

(2R,4aR,6S,7S,8R,8aR)-8-Benzyloxy-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-ol; In dichloromethane; at -60 - 20 ℃; for 3.5h; Further stages.;
DOI:10.1021/ol0340890

Reference yield:

: methyl 3-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside

: 503065-97-2
phenyl 4-O-benzoyl-3-O-benzyl-2-O-(2-trifluoromethylbenzenesulfonyl)-1-thio-β-L-rhamnopyranoside

: 503066-02-2
methyl 3-O-benzyl-4,6-O-benzylidene-2-O-[(4-O-benzoyl-3-O-benzyl-2-O-(2-trifluoromethylbenzenesulfonyl)-β-L-rhamnopyranosyl)]-α-D-mannopyranoside

: methyl 3-O-benzyl-4,6-O-benzylidene-2-O-[(4-O-benzoyl-3-O-benzyl-2-O-(2-trifluoromethylbenzenesulfonyl)-α-L-rhamnopyranosyl)]-α-D-mannopyranoside

Guidance literature:: phenyl 4-O-benzoyl-3-O-benzyl-2-O-(2-trifluoromethylbenzenesulfonyl)-1-thio-β-L-rhamnopyranoside; With 1-benzenesulfinyl piperidine; trifluoromethylsulfonic anhydride; 2,4,6-tri-tert-butylpyrimidine; In dichloromethane; acetonitrile; at -60 ℃; for 1h;

methyl 3-O-benzyl-4,6-O-benzylidene-α-D-mannopyranoside; In dichloromethane; acetonitrile; at -60 ℃; for 3h;
DOI:10.1016/j.carres.2006.03.036