3,4-Dichlorphenylmercaptoessigsaeurechlorid

Base Information

Chemical Name:3,4-Dichlorphenylmercaptoessigsaeurechlorid
CAS No.:53894-46-5
Molecular Formula:C₈H₅Cl₃OS
Molecular Weight:255.552
Hs Code.:

Synonyms:3,4-Dichlorphenylmercaptoessigsaeurechlorid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,4-Dichlorphenylmercaptoessigsaeurechlorid

Chemical Property:

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Technology Process of 3,4-Dichlorphenylmercaptoessigsaeurechlorid

There total 1 articles about 3,4-Dichlorphenylmercaptoessigsaeurechlorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21248-51-1
[(3,4-dichlorophenyl)thio]acetic acid

: 53894-46-5
3,4-Dichlorphenylmercaptoessigsaeurechlorid

Guidance literature:: With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1016/j.bmcl.2021.127846

Reference yield:

: 53894-46-5
3,4-Dichlorphenylmercaptoessigsaeurechlorid

: 115893-62-4
(3,4-dichloro-phenylsulfanyl)-acetic acid amide

Guidance literature:: With ammonia; In tetrahydrofuran; at 20 ℃; for 12h;
DOI:10.1016/j.bmcl.2021.127846

Reference yield:

: 53894-46-5
3,4-Dichlorphenylmercaptoessigsaeurechlorid

: C₁₁H₇Cl₂NO₂S₂

Guidance literature:: Multi-step reaction with 4 steps

1: ammonia / tetrahydrofuran / 12 h / 20 °C

2: Lawessons reagent / tetrahydrofuran / 12 h / 80 °C

3: ethanol / 6 h / 80 °C

4: lithium hydroxide monohydrate / tetrahydrofuran; methanol / 12 h / 80 °C

With Lawessons reagent; lithium hydroxide monohydrate; ammonia; In tetrahydrofuran; methanol; ethanol;
DOI:10.1016/j.bmcl.2021.127846