(Ph₂Si(CH₂PPh₂)2)PtMe₂

Base Information

• Chemical Name: (Ph₂Si(CH₂PPh₂)2)PtMe₂
• CAS No.: 577785-23-0
• Molecular Formula: C₄₀H₄₀P₂PtSi
• Molecular Weight: 805.871

Synonyms:(Ph₂Si(CH₂PPh₂)2)PtMe₂

Chemical Property of (Ph₂Si(CH₂PPh₂)2)PtMe₂

Chemical Property:

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Technology Process of (Ph₂Si(CH₂PPh₂)2)PtMe₂

There total 1 articles about (Ph₂Si(CH₂PPh₂)2)PtMe₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.6%

(1,5-cyclooctadiene)dimethylplatinum(II) + [Ph2Si(CH2PPh2)] (577785-19-4) → (Ph2Si(CH2PPh2)2)PtMe2 (577785-23-0)

Guidance literature:

In tetrahydrofuran; under inert atm. (COD)PtMe2 and (Ph2Si(CH2PPh2)2) were mixed in THF and stirred for 30 min; react. mixt. was concd. under reduced pressure and triturated with pentane, residue was dried in vacuo; elem. anal.;

DOI:10.1021/ja0296071

Reference yield: 93.8%

tetrahydrofuran (109-99-9,24979-97-3,77392-70-2) + [H(OEt2)2][B(C6F5)4] + (Ph2Si(CH2PPh2)2)PtMe2 (577785-23-0) → [(Ph2Si(CH2PPh2)2)Pt(Me)(THF)][B(C6F5)4] (577785-30-9)

Guidance literature:

In tetrahydrofuran; dichloromethane; under inert atm. to soln. (Ph2Si(CH2PPh2)2)PtMe2 in CH2Cl2-THF soln. (H(Et2O)2)(B(C6F5)4) in CH2Cl2 was added and stirred for 10 min; volatiles were removed under reduced pressure, triturated and washed with petroleum ether, and dried in vacuo; elem. anal.;

DOI:10.1021/ja0296071

upstream raw materials:

[Ph₂Si(CH₂PPh₂)]

Downstream raw materials:

[(Ph₂Si(CH₂PPh₂)2)Pt(Me)(THF)][B(C₆F₅)4]

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