2-bromo-4-methoxy-5-(4-methoxybenzyloxy)-benzylacetate

Base Information

Chemical Name:2-bromo-4-methoxy-5-(4-methoxybenzyloxy)-benzylacetate
CAS No.:125145-48-4
Molecular Formula:C₁₈H₁₉BrO₅
Molecular Weight:395.25
Hs Code.:

Synonyms:2-bromo-4-methoxy-5-(4-methoxybenzyloxy)-benzylacetate

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Chemical Property of 2-bromo-4-methoxy-5-(4-methoxybenzyloxy)-benzylacetate

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Technology Process of 2-bromo-4-methoxy-5-(4-methoxybenzyloxy)-benzylacetate

There total 5 articles about 2-bromo-4-methoxy-5-(4-methoxybenzyloxy)-benzylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 72785-28-5
4-methoxy-5-(4-methoxybenzyloxy)-benzyl acetate

: 125145-48-4
2-bromo-4-methoxy-5-(4-methoxybenzyloxy)-benzylacetate

Guidance literature:: With bromine; sodium acetate; In acetic acid; for 1h; Ambient temperature; addition of bromine at 15 deg C;
DOI:10.1016/S0040-4020(01)81012-7

Reference yield:

: 621-59-0
isovanillin

: 125145-48-4
2-bromo-4-methoxy-5-(4-methoxybenzyloxy)-benzylacetate

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / anhydrous potassium carbonate / dimethylformamide / 2 h / 100 °C

2: 96 percent / sodium borohydride / ethanol / 1 h / Ambient temperature

3: 95 percent / pyridine / 0.5 h / Ambient temperature; addition of reagent at ice-bath cooling

4: 94 percent / sodium acetate, bromine / acetic acid / 1 h / Ambient temperature; addition of bromine at 15 deg C

With sodium tetrahydroborate; bromine; sodium acetate; potassium carbonate; In pyridine; ethanol; acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)81012-7

Reference yield:

: 72785-29-6
4-methoxy-3-((4-methoxybenzyl)oxy)benzaldehyde

: 125145-48-4
2-bromo-4-methoxy-5-(4-methoxybenzyloxy)-benzylacetate

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / sodium borohydride / ethanol / 1 h / Ambient temperature

2: 95 percent / pyridine / 0.5 h / Ambient temperature; addition of reagent at ice-bath cooling

3: 94 percent / sodium acetate, bromine / acetic acid / 1 h / Ambient temperature; addition of bromine at 15 deg C

With sodium tetrahydroborate; bromine; sodium acetate; In pyridine; ethanol; acetic acid;
DOI:10.1016/S0040-4020(01)81012-7