6'-formyl-4',5'-dehydro-4'-deoxy-6,3',2'',5'',3''',4'''-hexa-O-methoxycarbonyl-per-N-Cbz-paromomycin

Base Information

Chemical Name:6'-formyl-4',5'-dehydro-4'-deoxy-6,3',2'',5'',3''',4'''-hexa-O-methoxycarbonyl-per-N-Cbz-paromomycin
CAS No.:1284216-86-9
Molecular Formula:C₇₅H₈₃N₅O₃₅
Molecular Weight:1614.5
Hs Code.:

Synonyms:6'-formyl-4',5'-dehydro-4'-deoxy-6,3',2'',5'',3''',4'''-hexa-O-methoxycarbonyl-per-N-Cbz-paromomycin

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Chemical Property of 6'-formyl-4',5'-dehydro-4'-deoxy-6,3',2'',5'',3''',4'''-hexa-O-methoxycarbonyl-per-N-Cbz-paromomycin

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Technology Process of 6'-formyl-4',5'-dehydro-4'-deoxy-6,3',2'',5'',3''',4'''-hexa-O-methoxycarbonyl-per-N-Cbz-paromomycin

There total 1 articles about 6'-formyl-4',5'-dehydro-4'-deoxy-6,3',2'',5'',3''',4'''-hexa-O-methoxycarbonyl-per-N-Cbz-paromomycin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1284216-83-6
4'-O-mesyl-6,3',2'',5'',3''', 4'''-hexa-O-methoxycarbonyl-per-N-Cbz-paromomycin

: 1284216-86-9
6'-formyl-4',5'-dehydro-4'-deoxy-6,3',2'',5'',3''',4'''-hexa-O-methoxycarbonyl-per-N-Cbz-paromomycin

Guidance literature:: With sulfur trioxide pyridine complex; triethylamine; In dichloromethane; dimethyl sulfoxide; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol2027703

Reference yield: 97.0%

: 1284216-86-9
6'-formyl-4',5'-dehydro-4'-deoxy-6,3',2'',5'',3''',4'''-hexa-O-methoxycarbonyl-per-N-Cbz-paromomycin

: 1284216-87-0
6'-formyl-4',5'-dehydro-3',4'-dideoxy-6,3',2'',5'',3''',4'''-hexa-O-methoxycarbonyl-per-N-Cbz-paromomycin

Guidance literature:: With formic acid; triethylamine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tributylphosphine; In tetrahydrofuran; at 60 ℃; for 3h;

Reference yield:

: 1284216-86-9
6'-formyl-4',5'-dehydro-4'-deoxy-6,3',2'',5'',3''',4'''-hexa-O-methoxycarbonyl-per-N-Cbz-paromomycin

: 1284216-97-2
C₆₃H₇₁N₅O₂₃

Guidance literature:: 6'-formyl-4',5'-dehydro-4'-deoxy-6,3',2'',5'',3''',4'''-hexa-O-methoxycarbonyl-per-N-Cbz-paromomycin; With sodium methylate; In methanol; at 20 ℃; for 5h; pH=~ 8;

With acetic acid; In methanol;