(2R,3S)-3-hydroxy-2-({[(5-phenylpentyl)oxy]carbonyl}amino)butanoic acid

Base Information

Chemical Name:(2R,3S)-3-hydroxy-2-({[(5-phenylpentyl)oxy]carbonyl}amino)butanoic acid
CAS No.:1373157-00-6
Molecular Formula:C₁₆H₂₃NO₅
Molecular Weight:309.362
Hs Code.:

Synonyms:(2R,3S)-3-hydroxy-2-({[(5-phenylpentyl)oxy]carbonyl}amino)butanoic acid

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Chemical Property of (2R,3S)-3-hydroxy-2-({[(5-phenylpentyl)oxy]carbonyl}amino)butanoic acid

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Technology Process of (2R,3S)-3-hydroxy-2-({[(5-phenylpentyl)oxy]carbonyl}amino)butanoic acid

There total 2 articles about (2R,3S)-3-hydroxy-2-({[(5-phenylpentyl)oxy]carbonyl}amino)butanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10521-91-2
5-phenylpentan-1-ol

: 1373157-00-6
(2R,3S)-3-hydroxy-2-({[(5-phenylpentyl)oxy]carbonyl}amino)butanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / toluene / 92 h / 0 - 20 °C

2: tetrabutylammomium bromide; sodium hydrogencarbonate / tetrahydrofuran; water / 18 h / 20 °C

With pyridine; tetrabutylammomium bromide; sodium hydrogencarbonate; In tetrahydrofuran; water; toluene;
DOI:10.1021/jm300349j

Reference yield:

: 2270-20-4
5-Phenylpentanoic acid

: 1373157-00-6
(2R,3S)-3-hydroxy-2-({[(5-phenylpentyl)oxy]carbonyl}amino)butanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium aluminium tetrahydride / diethyl ether / 4 h / 0 °C / Inert atmosphere

1.2: 1 h / 0 °C / Inert atmosphere

2.1: pyridine / toluene / 2 h / 0 °C / Inert atmosphere

2.2: 16.5 h / 20 °C / Inert atmosphere

3.1: sodium hydrogencarbonate; tetrabutylammomium bromide / tetrahydrofuran; water / 18 h / 20 °C

With pyridine; lithium aluminium tetrahydride; tetrabutylammomium bromide; sodium hydrogencarbonate; In tetrahydrofuran; diethyl ether; water; toluene;

Reference yield: 45.0%

: 1373157-00-6
(2R,3S)-3-hydroxy-2-({[(5-phenylpentyl)oxy]carbonyl}amino)butanoic acid

: 1373625-34-3
(2S,3R)-2-methyl-4-oxo-3-oxetanylcarbamic acid 5-phenylpentyl ester

Guidance literature:: With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; In dichloromethane; at 0 - 20 ℃; for 19h; Inert atmosphere;
DOI:10.1021/ml300056y