ethyl 4-(3-[(2,4-dichlorobenzyl)amino]-5-methyl-4-{[(methylamino)carbonothioyl]amino}phenoxy)butanoate

Base Information

Chemical Name:ethyl 4-(3-[(2,4-dichlorobenzyl)amino]-5-methyl-4-{[(methylamino)carbonothioyl]amino}phenoxy)butanoate
CAS No.:808743-89-7
Molecular Formula:C₂₂H₂₇Cl₂N₃O₃S
Molecular Weight:484.447
Hs Code.:

Synonyms:ethyl 4-(3-[(2,4-dichlorobenzyl)amino]-5-methyl-4-{[(methylamino)carbonothioyl]amino}phenoxy)butanoate

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Chemical Property of ethyl 4-(3-[(2,4-dichlorobenzyl)amino]-5-methyl-4-{[(methylamino)carbonothioyl]amino}phenoxy)butanoate

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Technology Process of ethyl 4-(3-[(2,4-dichlorobenzyl)amino]-5-methyl-4-{[(methylamino)carbonothioyl]amino}phenoxy)butanoate

There total 9 articles about ethyl 4-(3-[(2,4-dichlorobenzyl)amino]-5-methyl-4-{[(methylamino)carbonothioyl]amino}phenoxy)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 808743-88-6
ethyl 4-{4-amino-3-[(2,4-dichlorobenzyl)amino]-5-methylphenoxy}butanoate

: 556-61-6
methyl thioisocyanate

: 808743-89-7
ethyl 4-(3-[(2,4-dichlorobenzyl)amino]-5-methyl-4-{[(methylamino)carbonothioyl]amino}phenoxy)butanoate

Guidance literature:: In ethanol; at 20 - 60 ℃; for 4h;

Reference yield:

: 808743-58-0
4-(4-amino-3-methyl-5-nitrophenoxy)butanoic acid

: 808743-89-7
ethyl 4-(3-[(2,4-dichlorobenzyl)amino]-5-methyl-4-{[(methylamino)carbonothioyl]amino}phenoxy)butanoate

Guidance literature:: Multi-step reaction with 6 steps

1.1: sulfuric acid / 13 h / 20 °C / Heating / reflux

2.1: sodium hydride / DMF (N,N-dimethyl-formamide) / 0.5 h / 0 - 20 °C

2.2: 3 h / 20 °C

3.1: hydrogen / palladium 10% on activated carbon / ethanol / 3 h / 20 °C / 760.05 Torr

4.1: potassium carbonate; sodium iodide / DMF (N,N-dimethyl-formamide) / 5 h / 80 °C

5.1: hydrogenchloride / 1,4-dioxane; ethanbol / 14 h / 20 °C

6.1: ethanol / 4 h / 20 - 60 °C

With hydrogenchloride; sulfuric acid; hydrogen; sodium hydride; potassium carbonate; sodium iodide; palladium 10% on activated carbon; In 1,4-dioxane; DMF (N,N-dimethyl-formamide); ethanbol; ethanol;

Reference yield:

: 808743-59-1
ethyl 4-(4-amino-3-methyl-5-nitrophenoxy)butanoate

: 808743-89-7
ethyl 4-(3-[(2,4-dichlorobenzyl)amino]-5-methyl-4-{[(methylamino)carbonothioyl]amino}phenoxy)butanoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / DMF (N,N-dimethyl-formamide) / 0.5 h / 0 - 20 °C

1.2: 3 h / 20 °C

2.1: hydrogen / palladium 10% on activated carbon / ethanol / 3 h / 20 °C / 760.05 Torr

3.1: potassium carbonate; sodium iodide / DMF (N,N-dimethyl-formamide) / 5 h / 80 °C

4.1: hydrogenchloride / 1,4-dioxane; ethanbol / 14 h / 20 °C

5.1: ethanol / 4 h / 20 - 60 °C

With hydrogenchloride; hydrogen; sodium hydride; potassium carbonate; sodium iodide; palladium 10% on activated carbon; In 1,4-dioxane; DMF (N,N-dimethyl-formamide); ethanbol; ethanol;