methyl 2-<2-oxo-3β-(diphenylacetyl)amino-4-(benzothiazol-2-yldithio)azetidin-1-yl>-2-(prop-2-en-2-yl)acetate

Base Information

Chemical Name:methyl 2-<2-oxo-3β-(diphenylacetyl)amino-4-(benzothiazol-2-yldithio)azetidin-1-yl>-2-(prop-2-en-2-yl)acetate
CAS No.:107908-32-7
Molecular Formula:C₃₂H₂₉N₃O₅S₃
Molecular Weight:631.797
Hs Code.:

Synonyms:methyl 2-<2-oxo-3β-(diphenylacetyl)amino-4-(benzothiazol-2-yldithio)azetidin-1-yl>-2-(prop-2-en-2-yl)acetate

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Chemical Property of methyl 2-<2-oxo-3β-(diphenylacetyl)amino-4-(benzothiazol-2-yldithio)azetidin-1-yl>-2-(prop-2-en-2-yl)acetate

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Technology Process of methyl 2-<2-oxo-3β-(diphenylacetyl)amino-4-(benzothiazol-2-yldithio)azetidin-1-yl>-2-(prop-2-en-2-yl)acetate

There total 1 articles about methyl 2-<2-oxo-3β-(diphenylacetyl)amino-4-(benzothiazol-2-yldithio)azetidin-1-yl>-2-(prop-2-en-2-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 149-30-4,118090-09-8
2-Mercaptobenzothiazole

: 101760-75-2
6β-(diphenylacetyl)aminopenicillanate 1R-sulfoxide

: 107908-32-7
methyl 2-<2-oxo-3β-(diphenylacetyl)amino-4-(benzothiazol-2-yldithio)azetidin-1-yl>-2-(prop-2-en-2-yl)acetate

Guidance literature:: In benzene; for 2h; Heating;

Reference yield: 77.0%

: 107908-32-7
methyl 2-<2-oxo-3β-(diphenylacetyl)amino-4-(benzothiazol-2-yldithio)azetidin-1-yl>-2-(prop-2-en-2-yl)acetate

: 2-((1R,6R)-3,8-Dioxo-4-phenyl-2-phenylacetyl-5-thia-2,7-diaza-bicyclo[4.2.0]oct-7-yl)-3-methyl-but-2-enoic acid methyl ester

Guidance literature:: With triethylamine; In dichloromethane; for 2h;

Reference yield:

: 107908-32-7
methyl 2-<2-oxo-3β-(diphenylacetyl)amino-4-(benzothiazol-2-yldithio)azetidin-1-yl>-2-(prop-2-en-2-yl)acetate

: 3-Methyl-2-((1R,4R,5R,6R)-3,5,8-trioxo-4-phenyl-2-phenylacetyl-5λ⁴-thia-2,7-diaza-bicyclo[4.2.0]oct-7-yl)-but-2-enoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / Et₃N / CH₂Cl₂ / 2 h

2: 78 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 1 h / 0 °C

With triethylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;