4-((1E)-2-{4-[(1E)-2-(4-formyl-2,5-dihexyloxyphenyl)vinyl]phenyl}vinyl)-2,5-dihexyloxybenzaldehyde

Base Information

Chemical Name:4-((1E)-2-{4-[(1E)-2-(4-formyl-2,5-dihexyloxyphenyl)vinyl]phenyl}vinyl)-2,5-dihexyloxybenzaldehyde
CAS No.:561062-57-5
Molecular Formula:C₄₈H₆₆O₆
Molecular Weight:739.048
Hs Code.:

Synonyms:4-((1E)-2-{4-[(1E)-2-(4-formyl-2,5-dihexyloxyphenyl)vinyl]phenyl}vinyl)-2,5-dihexyloxybenzaldehyde

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Chemical Property of 4-((1E)-2-{4-[(1E)-2-(4-formyl-2,5-dihexyloxyphenyl)vinyl]phenyl}vinyl)-2,5-dihexyloxybenzaldehyde

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Technology Process of 4-((1E)-2-{4-[(1E)-2-(4-formyl-2,5-dihexyloxyphenyl)vinyl]phenyl}vinyl)-2,5-dihexyloxybenzaldehyde

There total 4 articles about 4-((1E)-2-{4-[(1E)-2-(4-formyl-2,5-dihexyloxyphenyl)vinyl]phenyl}vinyl)-2,5-dihexyloxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 561062-55-3
C₅₂H₇₄O₈

: 561062-57-5
4-((1E)-2-{4-[(1E)-2-(4-formyl-2,5-dihexyloxyphenyl)vinyl]phenyl}vinyl)-2,5-dihexyloxybenzaldehyde

Guidance literature:: With hydrogenchloride; In chloroform; water; at 20 ℃; for 5h;
DOI:10.1021/jo026907s

Reference yield:

: 52577-04-5
p-xylylene-α,α'-bis(phosphonic acid dimethyl ester)

: 561062-57-5
4-((1E)-2-{4-[(1E)-2-(4-formyl-2,5-dihexyloxyphenyl)vinyl]phenyl}vinyl)-2,5-dihexyloxybenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: NaH / tetrahydrofuran / 4 h / 40 °C

2: 0.56 g / HCl / H₂O; CHCl₃ / 5 h / 20 °C

With hydrogenchloride; sodium hydride; In tetrahydrofuran; chloroform; water; 1: Horner-Wadsworth-Emmons reaction;
DOI:10.1021/jo026907s

Reference yield:

: 151903-52-5
1,4-bis(hexyloxy)benzene-2,5-dicarbaldehyde

: 561062-57-5
4-((1E)-2-{4-[(1E)-2-(4-formyl-2,5-dihexyloxyphenyl)vinyl]phenyl}vinyl)-2,5-dihexyloxybenzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / p-toluenesulfonic acid / toluene / 12 h / Heating

2: NaH / tetrahydrofuran / 4 h / 40 °C

3: 0.56 g / HCl / H₂O; CHCl₃ / 5 h / 20 °C

With hydrogenchloride; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; chloroform; water; toluene; 2: Horner-Wadsworth-Emmons reaction;
DOI:10.1021/jo026907s