(3S)-ethyl 1-(1-hydroxy-1-(4-((Z)-N'-hydroxycarbamimidoyl)phenyl)-2-methylpropan-2-yl)piperidine-3-carboxylate

Base Information

Chemical Name:(3S)-ethyl 1-(1-hydroxy-1-(4-((Z)-N'-hydroxycarbamimidoyl)phenyl)-2-methylpropan-2-yl)piperidine-3-carboxylate
CAS No.:1265750-13-7
Molecular Formula:C₁₉H₂₉N₃O₄
Molecular Weight:363.457
Hs Code.:

Synonyms:(3S)-ethyl 1-(1-hydroxy-1-(4-((Z)-N'-hydroxycarbamimidoyl)phenyl)-2-methylpropan-2-yl)piperidine-3-carboxylate

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Chemical Property of (3S)-ethyl 1-(1-hydroxy-1-(4-((Z)-N'-hydroxycarbamimidoyl)phenyl)-2-methylpropan-2-yl)piperidine-3-carboxylate

Chemical Property:

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Technology Process of (3S)-ethyl 1-(1-hydroxy-1-(4-((Z)-N'-hydroxycarbamimidoyl)phenyl)-2-methylpropan-2-yl)piperidine-3-carboxylate

There total 5 articles about (3S)-ethyl 1-(1-hydroxy-1-(4-((Z)-N'-hydroxycarbamimidoyl)phenyl)-2-methylpropan-2-yl)piperidine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₉H₂₆N₂O₃

: 1265750-13-7
(3S)-ethyl 1-(1-hydroxy-1-(4-((Z)-N'-hydroxycarbamimidoyl)phenyl)-2-methylpropan-2-yl)piperidine-3-carboxylate

Guidance literature:: With hydroxylamine hydrochloride; sodium hydrogencarbonate; In isopropyl alcohol; at 75 ℃;

Reference yield:

: 4-(1-hydroxy-2-methylpropyl)-benzonitrile

: 1265750-13-7
(3S)-ethyl 1-(1-hydroxy-1-(4-((Z)-N'-hydroxycarbamimidoyl)phenyl)-2-methylpropan-2-yl)piperidine-3-carboxylate

Guidance literature:: Multi-step reaction with 5 steps

1: Dess-Martin periodane / dichloromethane / 2 h

2: bromine; acetic acid / 72 h

3: sodium iodide / dimethyl sulfoxide / 90 °C

4: sodium tetrahydroborate / methanol / 1 h

5: hydroxylamine hydrochloride; sodium hydrogencarbonate / isopropyl alcohol / 75 °C

With sodium tetrahydroborate; hydroxylamine hydrochloride; bromine; sodium hydrogencarbonate; Dess-Martin periodane; acetic acid; sodium iodide; In methanol; dichloromethane; dimethyl sulfoxide; isopropyl alcohol;

Reference yield:

: 1265323-78-1
4-(2-bromo-2-methylpropanoyl)benzonitrile

: 1265750-13-7
(3S)-ethyl 1-(1-hydroxy-1-(4-((Z)-N'-hydroxycarbamimidoyl)phenyl)-2-methylpropan-2-yl)piperidine-3-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium iodide / dimethyl sulfoxide / 90 °C

2: sodium tetrahydroborate / methanol / 1 h

3: hydroxylamine hydrochloride; sodium hydrogencarbonate / isopropyl alcohol / 75 °C

With sodium tetrahydroborate; hydroxylamine hydrochloride; sodium hydrogencarbonate; sodium iodide; In methanol; dimethyl sulfoxide; isopropyl alcohol;