{triethylammonium}{closo-3-(triphenylphosphine)-3,3-(Cl)2-3,1,2-RhC₂B₉H₁₁}

Base Information

Chemical Name:{triethylammonium}{closo-3-(triphenylphosphine)-3,3-(Cl)2-3,1,2-RhC₂B₉H₁₁}
CAS No.:87226-27-5
Molecular Formula:C₈H₂₀N*C₂₀H₂₆B₉Cl₂PRh
Molecular Weight:698.764
Hs Code.:

{triethylammonium}{closo-3-(triphenylphosphine)-3,3-(Cl)2-3,1,2-RhC<sub>2</sub>B<sub>9</sub>H<sub>11</sub>}

Synonyms:{triethylammonium}{closo-3-(triphenylphosphine)-3,3-(Cl)2-3,1,2-RhC₂B₉H₁₁}

Suppliers and Price of {triethylammonium}{closo-3-(triphenylphosphine)-3,3-(Cl)2-3,1,2-RhC₂B₉H₁₁}

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {triethylammonium}{closo-3-(triphenylphosphine)-3,3-(Cl)2-3,1,2-RhC₂B₉H₁₁}

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Technology Process of {triethylammonium}{closo-3-(triphenylphosphine)-3,3-(Cl)2-3,1,2-RhC₂B₉H₁₁}

There total 2 articles about {triethylammonium}{closo-3-(triphenylphosphine)-3,3-(Cl)2-3,1,2-RhC₂B₉H₁₁} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 85369-53-5
{triethylammonium}{closo-3-(triphenylphosphine)-3-(carbonyl)-3,1,2-RhC₂B₉H₁₁}

: 87226-27-5
{triethylammonium}{closo-3-(triphenylphosphine)-3,3-(Cl)2-3,1,2-RhC₂B₉H₁₁}

Guidance literature:: With benzhydroxamic acid chloride; CH₂Cl₂; In dichloromethane; acetone; under N2 or Ar, cycloadduct formed between Rh complex and benzhydroxamic acid chloride (prepd. by method of Walker, J. A.; Knobler, C. B.; Hawthorne, M. F. J. Am. Chem. Soc. 1983, 105, 3370) dissolved in CH2Cl2 and acetone, stirred for 3 h at room temp.; benzene added, concd. in vac., crystals filtered off, rinsed with pentane, recrystd. from acetone/heptane; elem. anal.;