C₁₆H₂₂O₄

Base Information

Chemical Name:C₁₆H₂₂O₄
CAS No.:952496-54-7
Molecular Formula:C₁₆H₂₂O₄
Molecular Weight:278.348
Hs Code.:

C<sub>16</sub>H<sub>22</sub>O<sub>4</sub>

Synonyms:C₁₆H₂₂O₄

Suppliers and Price of C₁₆H₂₂O₄

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₆H₂₂O₄

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₆H₂₂O₄

There total 9 articles about C₁₆H₂₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 952496-53-6
C₁₆H₂₄O₄

: 952496-54-7
C₁₆H₂₂O₄

Guidance literature:: With pyridine-SO₃ complex; TEA; dimethyl sulfoxide; In dichloromethane; at 20 ℃; for 0.5h;
DOI:10.1016/j.tet.2007.07.005

Reference yield:

: 919608-47-2
5-(2,2-dimethyl-[1,3]dioxolan-4-yl)-2-methyl-pentane-1,3-diol

: 952496-54-7
C₁₆H₂₂O₄

Guidance literature:: Multi-step reaction with 7 steps

1: 3.59 g / imidazole / CH₂Cl₂ / 1 h / 20 °C

2: 98 percent / TEA / CH₂Cl₂ / 0 - 20 °C

3: 84 percent / CSA; methanol / 2 h / 20 °C

4: 80 percent / sodium hexamethyldisilazide / tetrahydrofuran / 0 - 20 °C

5: 67 percent / sodium hexamethyldisilazide; TBAI / tetrahydrofuran; dimethylformamide / 0 - 20 °C

6: 93 percent / TBAF / tetrahydrofuran / 12 h / 20 °C

7: 78 percent / SO₃*pyridine; TEA; DMSO / CH₂Cl₂ / 0.5 h / 20 °C

With 1H-imidazole; methanol; pyridine-SO₃ complex; TEA; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; sodium hexamethyldisilazane; tetra-(n-butyl)ammonium iodide; dimethyl sulfoxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 4: Williamson ether synthesis;
DOI:10.1016/j.tet.2007.07.005

Reference yield:

: 919608-28-9
3-[5-(2,2-dimethyl-[1,3]dioxolan-4-yl)-3-hydroxy-2-methyl-pentanoyl]-4-methyl-5-phenyl-oxazolidin-2-one

: 952496-54-7
C₁₆H₂₂O₄

Guidance literature:: Multi-step reaction with 8 steps

1: lithium borohydride / diethyl ether; tetrahydrofuran / 0 - 20 °C

2: 3.59 g / imidazole / CH₂Cl₂ / 1 h / 20 °C

3: 98 percent / TEA / CH₂Cl₂ / 0 - 20 °C

4: 84 percent / CSA; methanol / 2 h / 20 °C

5: 80 percent / sodium hexamethyldisilazide / tetrahydrofuran / 0 - 20 °C

6: 67 percent / sodium hexamethyldisilazide; TBAI / tetrahydrofuran; dimethylformamide / 0 - 20 °C

7: 93 percent / TBAF / tetrahydrofuran / 12 h / 20 °C

8: 78 percent / SO₃*pyridine; TEA; DMSO / CH₂Cl₂ / 0.5 h / 20 °C

With 1H-imidazole; methanol; lithium borohydride; pyridine-SO₃ complex; TEA; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; sodium hexamethyldisilazane; tetra-(n-butyl)ammonium iodide; dimethyl sulfoxide; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide; 5: Williamson ether synthesis;
DOI:10.1016/j.tet.2007.07.005