Technology Process of C34H42FN3O10
There total 17 articles about C34H42FN3O10 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium carbonate;
In
1,4-dioxane; water;
at 20 ℃;
for 15h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tetrakis(triphenylphosphine) palladium(0); 1,3-dimethylbarbituric acid / dichloromethane; ethyl acetate / 2 h / 20 °C
2: sodium carbonate / water; 1,4-dioxane / 15 h / 0 - 20 °C
With
tetrakis(triphenylphosphine) palladium(0); 1,3-dimethylbarbituric acid; sodium carbonate;
In
1,4-dioxane; dichloromethane; water; ethyl acetate;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: oxalyl dichloride / dichloromethane / 0.25 h / 20 °C
2: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 16 h / 0 - 20 °C
3: 1-amino-3-(dimethylamino)propane / tetrahydrofuran / 0 - 20 °C
4: triphenylphosphine; 1,1'-azodicarbonyl-dipiperidine / chloroform / 19 h / 0 - 20 °C
5: tetrakis(triphenylphosphine) palladium(0); 1,3-dimethylbarbituric acid / dichloromethane; ethyl acetate / 2 h / 20 °C
6: sodium carbonate / water; 1,4-dioxane / 15 h / 0 - 20 °C
With
tetrakis(triphenylphosphine) palladium(0); oxalyl dichloride; 1,3-dimethylbarbituric acid; sodium carbonate; 1-amino-3-(dimethylamino)propane; N-ethyl-N,N-diisopropylamine; triphenylphosphine; 1,1'-azodicarbonyl-dipiperidine;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; chloroform; water; ethyl acetate;
4: |Mitsunobu Displacement;