(S)-2-(benzyloxycarbonylamino)-6-[(2-oxo-2H-chromen-3-ylcarbonyl)amino]hexanoic acid

Base Information

Chemical Name:(S)-2-(benzyloxycarbonylamino)-6-[(2-oxo-2H-chromen-3-ylcarbonyl)amino]hexanoic acid
CAS No.:1037657-49-0
Molecular Formula:C₂₄H₂₄N₂O₇
Molecular Weight:452.464
Hs Code.:

Synonyms:(S)-2-(benzyloxycarbonylamino)-6-[(2-oxo-2H-chromen-3-ylcarbonyl)amino]hexanoic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-(benzyloxycarbonylamino)-6-[(2-oxo-2H-chromen-3-ylcarbonyl)amino]hexanoic acid

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Technology Process of (S)-2-(benzyloxycarbonylamino)-6-[(2-oxo-2H-chromen-3-ylcarbonyl)amino]hexanoic acid

There total 1 articles about (S)-2-(benzyloxycarbonylamino)-6-[(2-oxo-2H-chromen-3-ylcarbonyl)amino]hexanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 312929-01-4
3-(1H-benzotriazol-1-ylcarbonyl)-2H-chromene-2-one

: 2212-75-1
N₂-[(benzyloxy)carbonyl]-L-lysine

: 1037657-49-0
(S)-2-(benzyloxycarbonylamino)-6-[(2-oxo-2H-chromen-3-ylcarbonyl)amino]hexanoic acid

Guidance literature:: With triethylamine; In water; acetonitrile; at 20 ℃; for 1h;
DOI:10.1055/s-2008-1067078

Reference yield: 79.0%

: 95-14-7,27556-51-0
1,2,3-Benzotriazole

: 1037657-49-0
(S)-2-(benzyloxycarbonylamino)-6-[(2-oxo-2H-chromen-3-ylcarbonyl)amino]hexanoic acid

: 1037657-51-4
benzyl {(S)-1-(1H-1,2,3-benzotriazol-1-ylcarbonyl)-5-[(2-oxo-2H-chromen-3-ylcarbonyl)amino]pentyl}carbamate

Guidance literature:: 1,2,3-Benzotriazole; With thionyl chloride; In dichloromethane; at 20 ℃; for 0.333333h;

(S)-2-(benzyloxycarbonylamino)-6-[(2-oxo-2H-chromen-3-ylcarbonyl)amino]hexanoic acid; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1055/s-2008-1067078