isothiocyanato-3-(n-perfluorooctyl)benzene

Base Information

• Chemical Name: isothiocyanato-3-(n-perfluorooctyl)benzene
• CAS No.: 120606-37-3
• Molecular Formula: C₁₅H₄F₁₇NS
• Molecular Weight: 553.242
• Mol file: 120606-37-3.mol

Synonyms:isothiocyanato-3-(n-perfluorooctyl)benzene

Chemical Property of isothiocyanato-3-(n-perfluorooctyl)benzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of isothiocyanato-3-(n-perfluorooctyl)benzene

There total 3 articles about isothiocyanato-3-(n-perfluorooctyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.7%

thiophosgene (463-71-8) + 3-(n-perfluorooctyl)aniline (119489-67-7) → isothiocyanato-3-(n-perfluorooctyl)benzene (120606-37-3)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 0 - 20 ℃; for 12.16h; Inert atmosphere;

DOI:10.1039/c3nj00807j

Reference yield:

1-iodoheptadecafluorooctane (507-63-1) → isothiocyanato-3-(n-perfluorooctyl)benzene (120606-37-3)

Guidance literature:

Multi-step reaction with 2 steps

1: Cu / dimethylformamide

With copper; In N,N-dimethyl-formamide;

DOI:10.1246/cl.1989.231

Reference yield:

3-Iodoaniline (626-01-7) → isothiocyanato-3-(n-perfluorooctyl)benzene (120606-37-3)

Guidance literature:

Multi-step reaction with 2 steps

1: Cu / dimethylformamide

With copper; In N,N-dimethyl-formamide;

DOI:10.1246/cl.1989.231

upstream raw materials:

thiophosgene

3-(n-perfluorooctyl)aniline

1-iodoheptadecafluorooctane

3-Iodoaniline