2,3,5-tri-O-acetyl-4-O,6-N-carbonyl-6-amino-6-deoxy-D-galactose N',N''-diphenylformazan

Base Information

Chemical Name:2,3,5-tri-O-acetyl-4-O,6-N-carbonyl-6-amino-6-deoxy-D-galactose N',N''-diphenylformazan
CAS No.:406218-01-7
Molecular Formula:C₂₅H₂₇N₅O₈
Molecular Weight:525.518
Hs Code.:

Synonyms:2,3,5-tri-O-acetyl-4-O,6-N-carbonyl-6-amino-6-deoxy-D-galactose N',N''-diphenylformazan

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Chemical Property of 2,3,5-tri-O-acetyl-4-O,6-N-carbonyl-6-amino-6-deoxy-D-galactose N',N''-diphenylformazan

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Technology Process of 2,3,5-tri-O-acetyl-4-O,6-N-carbonyl-6-amino-6-deoxy-D-galactose N',N''-diphenylformazan

There total 4 articles about 2,3,5-tri-O-acetyl-4-O,6-N-carbonyl-6-amino-6-deoxy-D-galactose N',N''-diphenylformazan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 108-24-7
acetic anhydride

: 406218-00-6
4-O,6-N-carbonyl-6-amino-6-deoxy-D-galactose N',N''-diphenylformazan

: 406218-01-7
2,3,5-tri-O-acetyl-4-O,6-N-carbonyl-6-amino-6-deoxy-D-galactose N',N''-diphenylformazan

Guidance literature:: With pyridine; at 0 ℃; for 48h;
DOI:10.1081/CAR-100108287

Reference yield:

: 59-88-1
phenylhydrazine hydrochloride

: 406218-01-7
2,3,5-tri-O-acetyl-4-O,6-N-carbonyl-6-amino-6-deoxy-D-galactose N',N''-diphenylformazan

Guidance literature:: Multi-step reaction with 3 steps

1: NaOAc*3H₂O / H₂O / 0 - 20 °C

2: pyridine / H₂O; ethanol / 0 - 20 °C

3: 63 percent / pyridine / 48 h / 0 °C

With pyridine; sodium acetate; In ethanol; water;
DOI:10.1081/CAR-100108287

Reference yield:

: 100639-16-5
6-amino-6-deoxy-α-D-galactopyranose 6,4-(cyclic carbamate)

: 406218-01-7
2,3,5-tri-O-acetyl-4-O,6-N-carbonyl-6-amino-6-deoxy-D-galactose N',N''-diphenylformazan

Guidance literature:: Multi-step reaction with 3 steps

1: NaOAc*3H₂O / H₂O / 0 - 20 °C

2: pyridine / H₂O; ethanol / 0 - 20 °C

3: 63 percent / pyridine / 48 h / 0 °C

With pyridine; sodium acetate; In ethanol; water;
DOI:10.1081/CAR-100108287