C₂₅H₃₀O₆

Base Information

Chemical Name:C₂₅H₃₀O₆
CAS No.:1572455-52-7
Molecular Formula:C₂₅H₃₀O₆
Molecular Weight:426.51
Hs Code.:

C<sub>25</sub>H<sub>30</sub>O<sub>6</sub>

Synonyms:C₂₅H₃₀O₆

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Chemical Property of C₂₅H₃₀O₆

Chemical Property:

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Technology Process of C₂₅H₃₀O₆

There total 16 articles about C₂₅H₃₀O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1572455-51-6
C₂₅H₃₂O₇

: 1572455-52-7
C₂₅H₃₀O₆

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 18 ℃; for 1.17h;
DOI:10.1021/jo500210k

Reference yield:

: 67451-62-1,82683-92-9,132958-32-8,130792-45-9
cis-(1S,2S)-1,2-dihydroxy-3-bromocyclohexa-3,5-diene

: 1572455-52-7
C₂₅H₃₀O₆

Guidance literature:: Multi-step reaction with 9 steps

1: N-Bromosuccinimide / water; tetrahydrofuran / 3 h / 18 °C

2: toluene-4-sulfonic acid / 2 h / 18 °C

3: methanol / 6 h / 0 - 18 °C

4: sodium hydride / tetrahydrofuran / 4.5 h / 0 - 18 °C

5: acetic acid / water / 14 h / 70 °C

6: toluene-4-sulfonic acid / dichloromethane / 2 h / 0 °C

7: diisobutylaluminium hydride / dichloromethane; hexane / 6 h / -78 °C / Inert atmosphere

8: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; triethylamine / water; tetrahydrofuran / 1.5 h / 70 °C / Inert atmosphere

9: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 1.17 h / 18 °C

With N-Bromosuccinimide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sodium hydride; diisobutylaluminium hydride; toluene-4-sulfonic acid; acetic acid; triethylamine; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol; hexane; dichloromethane; water; 8: |Suzuki-Miyaura Coupling;
DOI:10.1021/jo500210k

Reference yield:

: 1514823-92-7
C₈H₁₃BrO₄

: 1572455-52-7
C₂₅H₃₀O₆

Guidance literature:: Multi-step reaction with 4 steps

1: toluene-4-sulfonic acid / dichloromethane / 2 h / 0 °C

2: diisobutylaluminium hydride / dichloromethane; hexane / 6 h / -78 °C / Inert atmosphere

3: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; triethylamine / water; tetrahydrofuran / 1.5 h / 70 °C / Inert atmosphere

4: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 1.17 h / 18 °C

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; diisobutylaluminium hydride; toluene-4-sulfonic acid; triethylamine; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; hexane; dichloromethane; water; 3: |Suzuki-Miyaura Coupling;
DOI:10.1021/jo500210k