C₂₄H₂₅Cl₂F₃N₂O₅

Base Information

Chemical Name:C₂₄H₂₅Cl₂F₃N₂O₅
CAS No.:1206625-70-8
Molecular Formula:C₂₄H₂₅Cl₂F₃N₂O₅
Molecular Weight:549.374
Hs Code.:

C<sub>24</sub>H<sub>25</sub>Cl<sub>2</sub>F<sub>3</sub>N<sub>2</sub>O<sub>5</sub>

Synonyms:C₂₄H₂₅Cl₂F₃N₂O₅

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Chemical Property of C₂₄H₂₅Cl₂F₃N₂O₅

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Technology Process of C₂₄H₂₅Cl₂F₃N₂O₅

There total 7 articles about C₂₄H₂₅Cl₂F₃N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 945999-98-4
5-bromo-2-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]pyridine

: 1206625-70-8
C₂₄H₂₅Cl₂F₃N₂O₅

Guidance literature:: Multi-step reaction with 3 steps

1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / N,N-dimethyl acetamide / 20 h / 80 - 85 °C / Inert atmosphere; Large scale reaction

2: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium hydrogencarbonate / 2-methyltetrahydrofuran; water / 1 h / 60 °C / Inert atmosphere; Large scale reaction

3: tetrafluoroboric acid diethyl ether; [bis(2-methylallyl)cycloocta-1,5-diene]ruthenium(II); Josiphos SL-J₂₁₂-1; hydrogen / 2-methyltetrahydrofuran / 43 h / 23 °C / 51716.2 Torr / Autoclave sealed; Large scale reaction

With tetrafluoroboric acid diethyl ether; [bis(2-methylallyl)cycloocta-1,5-diene]ruthenium(II); dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; Josiphos SL-J₂₁₂-1; hydrogen; potassium acetate; potassium hydrogencarbonate; In 2-methyltetrahydrofuran; N,N-dimethyl acetamide; water;
DOI:10.1021/jo102070e

Reference yield:

: 1246643-49-1
C₁₀H₁₂F₃NO₄

: 1206625-70-8
C₂₄H₂₅Cl₂F₃N₂O₅

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 1.17 h / -10 °C / Inert atmosphere; Large scale reaction

2: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium hydrogencarbonate / 2-methyltetrahydrofuran; water / 1 h / 60 °C / Inert atmosphere; Large scale reaction

3: tetrafluoroboric acid diethyl ether; [bis(2-methylallyl)cycloocta-1,5-diene]ruthenium(II); Josiphos SL-J₂₁₂-1; hydrogen / 2-methyltetrahydrofuran / 43 h / 23 °C / 51716.2 Torr / Autoclave sealed; Large scale reaction

With tetrafluoroboric acid diethyl ether; [bis(2-methylallyl)cycloocta-1,5-diene]ruthenium(II); dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; Josiphos SL-J₂₁₂-1; hydrogen; potassium hydrogencarbonate; triethylamine; In 2-methyltetrahydrofuran; dichloromethane; water;
DOI:10.1021/jo102070e

Reference yield:

: 1206625-66-2
1-(2,2,2-trifluoro-acetyl)-4-trifluoromethanesulfonyloxy-1,2,5,6-tetrahydro-pyridine-3-carboxylic acid ethyl ester

: 1206625-70-8
C₂₄H₂₅Cl₂F₃N₂O₅

Guidance literature:: Multi-step reaction with 2 steps

1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium hydrogencarbonate / 2-methyltetrahydrofuran; water / 1 h / 60 °C / Inert atmosphere; Large scale reaction

2: tetrafluoroboric acid diethyl ether; [bis(2-methylallyl)cycloocta-1,5-diene]ruthenium(II); Josiphos SL-J₂₁₂-1; hydrogen / 2-methyltetrahydrofuran / 43 h / 23 °C / 51716.2 Torr / Autoclave sealed; Large scale reaction

With tetrafluoroboric acid diethyl ether; [bis(2-methylallyl)cycloocta-1,5-diene]ruthenium(II); dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; Josiphos SL-J₂₁₂-1; hydrogen; potassium hydrogencarbonate; In 2-methyltetrahydrofuran; water;
DOI:10.1021/jo102070e