2,3,4,6-tetra-O-benzyl-1-O-(N-benzyloxycarbonylglycylglycyl-D-phenylalanyl)-β-D-glucopyranose

Base Information

• Chemical Name: 2,3,4,6-tetra-O-benzyl-1-O-(N-benzyloxycarbonylglycylglycyl-D-phenylalanyl)-β-D-glucopyranose
• CAS No.: 75719-93-6
• Molecular Formula: C₅₅H₅₇N₃O₁₁
• Molecular Weight: 936.071

Synonyms:2,3,4,6-tetra-O-benzyl-1-O-(N-benzyloxycarbonylglycylglycyl-D-phenylalanyl)-β-D-glucopyranose

Chemical Property of 2,3,4,6-tetra-O-benzyl-1-O-(N-benzyloxycarbonylglycylglycyl-D-phenylalanyl)-β-D-glucopyranose

Chemical Property:

Purity/Quality:

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Technology Process of 2,3,4,6-tetra-O-benzyl-1-O-(N-benzyloxycarbonylglycylglycyl-D-phenylalanyl)-β-D-glucopyranose

There total 7 articles about 2,3,4,6-tetra-O-benzyl-1-O-(N-benzyloxycarbonylglycylglycyl-D-phenylalanyl)-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-benzyloxycarbonyl-L-glycyl-L-glycyl-L-phenylalanine (13171-93-2) → 2,3,4,6-tetra-O-benzyl-1-O-(N-benzyloxycarbonylglycylglycyl-L,D-phenylalanyl)-α-D-glucopyranose (75719-90-3,75719-91-4,75719-92-5,75719-93-6)

Guidance literature:

Multi-step reaction with 2 steps

1: dicyclohexylcarbodi-imide / dimethylformamide

2: imidazole / dimethylformamide / 48 h / Ambient temperature

With 1H-imidazole; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;

DOI:10.1016/S0008-6215(00)85517-2

Reference yield:

N-benzyloxycarbonyl-L-glycyl-L-glycyl-L-phenylalanine (13171-93-2) → 2,3,4,6-tetra-O-benzyl-1-O-(N-benzyloxycarbonylglycylglycyl-L,D-phenylalanyl)-β-D-glucopyranose (75719-90-3,75719-91-4,75719-92-5,75719-93-6)

Guidance literature:

Multi-step reaction with 2 steps

1: dicyclohexylcarbodi-imide / dimethylformamide

2: imidazole / dimethylformamide / 48 h / Ambient temperature

With 1H-imidazole; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;

DOI:10.1016/S0008-6215(00)85517-2

Reference yield:

N-benzyloxycarbonyl-L-glycyl-L-glycyl-L-phenylalanine (13171-93-2) → 2,3,4,6-tetra-O-benzyl-1-O-(N-benzyloxycarbonylglycylglycyl-D-phenylalanyl)-β-D-glucopyranose (75719-93-6)

Guidance literature:

Multi-step reaction with 2 steps

1: dicyclohexylcarbodi-imide / dimethylformamide

2: imidazole / dimethylformamide / 48 h / Ambient temperature

With 1H-imidazole; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;

DOI:10.1016/S0008-6215(00)85517-2

upstream raw materials:

2,3,4,6-tetra-O-benzyl-D-glucopyranose

N-benzyloxycarbonyl-glycylglycyl-L-phenylalanine pentachlorophenyl ester

N-benzyloxycarbonyl-L-glycyl-L-glycyl-L-phenylalanine

Downstream raw materials:

β-D-glucose

glycylglycine

L-phenylalanine

glycylglycyl-D-phenylalanine

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