C₁₇H₁₅BrO₄S

Base Information

Chemical Name:C₁₇H₁₅BrO₄S
CAS No.:1047664-14-1
Molecular Formula:C₁₇H₁₅BrO₄S
Molecular Weight:395.274
Hs Code.:

C<sub>17</sub>H<sub>15</sub>BrO<sub>4</sub>S

Synonyms:C₁₇H₁₅BrO₄S

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Chemical Property of C₁₇H₁₅BrO₄S

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Technology Process of C₁₇H₁₅BrO₄S

There total 4 articles about C₁₇H₁₅BrO₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1047664-13-0
C₁₉H₁₉BrO₄S

: 1047664-14-1
C₁₇H₁₅BrO₄S

Guidance literature:: dichloro(tricyclohexylphosphino)(benzylidene)(1,3-dimesityl-4,5-dihydroimidazol-2-ylidene)ruthenium(III); In dichloromethane; at 20 ℃; for 5h;

Reference yield:

: 811867-45-5
3-bromo-2-hydroxy styrene

: 1047664-14-1
C₁₇H₁₅BrO₄S

Guidance literature:: Multi-step reaction with 2 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0 °C / Inert atmosphere

2: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 20 °C / Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm2007062

Reference yield:

: 95-56-7
2-hydroxybromobenzene

: 1047664-14-1
C₁₇H₁₅BrO₄S

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine; magnesium chloride / acetonitrile / 20 - 90 °C / Inert atmosphere

2.1: potassium tert-butylate / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

2.2: -78 - 20 °C / Inert atmosphere

3.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0 °C / Inert atmosphere

4.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 20 °C / Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; di-isopropyl azodicarboxylate; potassium tert-butylate; triethylamine; triphenylphosphine; magnesium chloride; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/jm2007062