3-Methylbutansaeure-<9,11-dimethyl-4,6-bis(1-methylaethyl)-2,2-diphenyl-1,3-benzodioxolo<5,6-b><1,4>benzodioxin-7-yl>ester

Base Information

Chemical Name:3-Methylbutansaeure-<9,11-dimethyl-4,6-bis(1-methylaethyl)-2,2-diphenyl-1,3-benzodioxolo<5,6-b><1,4>benzodioxin-7-yl>ester
CAS No.:101958-91-2
Molecular Formula:C₃₈H₄₀O₆
Molecular Weight:592.732
Hs Code.:

Synonyms:3-Methylbutansaeure-<9,11-dimethyl-4,6-bis(1-methylaethyl)-2,2-diphenyl-1,3-benzodioxolo<5,6-b><1,4>benzodioxin-7-yl>ester

Suppliers and Price of 3-Methylbutansaeure-<9,11-dimethyl-4,6-bis(1-methylaethyl)-2,2-diphenyl-1,3-benzodioxolo<5,6-b><1,4>benzodioxin-7-yl>ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-Methylbutansaeure-<9,11-dimethyl-4,6-bis(1-methylaethyl)-2,2-diphenyl-1,3-benzodioxolo<5,6-b><1,4>benzodioxin-7-yl>ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-Methylbutansaeure-<9,11-dimethyl-4,6-bis(1-methylaethyl)-2,2-diphenyl-1,3-benzodioxolo<5,6-b><1,4>benzodioxin-7-yl>ester

There total 5 articles about 3-Methylbutansaeure-<9,11-dimethyl-4,6-bis(1-methylaethyl)-2,2-diphenyl-1,3-benzodioxolo<5,6-b><1,4>benzodioxin-7-yl>ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 101958-87-6
9,11-Dimethyl-4,6-bis(1-methylaethyl)-2,2-diphenyl-1,3-benzodioxolo<5,6-b><1,4>benzodioxin-7-ol

: 108-12-3
isopentanoyl chloride

: 101958-91-2
3-Methylbutansaeure-<9,11-dimethyl-4,6-bis(1-methylaethyl)-2,2-diphenyl-1,3-benzodioxolo<5,6-b><1,4>benzodioxin-7-yl>ester

Guidance literature:: With pyridine; at 8 ℃; for 48h;
DOI:10.1002/hlca.19850680407

Reference yield:

: 2051-90-3
Dichlorodiphenylmethane

: 101958-91-2
3-Methylbutansaeure-<9,11-dimethyl-4,6-bis(1-methylaethyl)-2,2-diphenyl-1,3-benzodioxolo<5,6-b><1,4>benzodioxin-7-yl>ester

Guidance literature:: Multi-step reaction with 3 steps

1: α-pinene / CHCl3 / 1.) 80 deg C, 12 h; 2.) 100 deg C, 24 h

2: 93 percent / LiAlH₄ / tetrahydrofuran / 8 h / 60 °C

3: 82 percent / pyridine / 48 h / 8 °C

With pyridine; lithium aluminium tetrahydride; Pinene; In tetrahydrofuran; chloroform;
DOI:10.1002/hlca.19850680407

Reference yield:

: 101958-81-0
Methanesulfonic acid 7,8-dihydroxy-1,9-diisopropyl-4,6-dimethyl-dibenzo[1,4]dioxin-2-yl ester

: 101958-91-2
3-Methylbutansaeure-<9,11-dimethyl-4,6-bis(1-methylaethyl)-2,2-diphenyl-1,3-benzodioxolo<5,6-b><1,4>benzodioxin-7-yl>ester

Guidance literature:: Multi-step reaction with 3 steps

1: α-pinene / CHCl3 / 1.) 80 deg C, 12 h; 2.) 100 deg C, 24 h

2: 93 percent / LiAlH₄ / tetrahydrofuran / 8 h / 60 °C

3: 82 percent / pyridine / 48 h / 8 °C

With pyridine; lithium aluminium tetrahydride; Pinene; In tetrahydrofuran; chloroform;
DOI:10.1002/hlca.19850680407